反应条件
Ir(indenyl)(cyclooctadiene); bis(dimethylphosphino)ethane in neat (no solvent) (N2); stirring a mixt. of 1,3-diisopropylbenzene, Ir complex, diphosphine and boron compd. at room temp. for 20 min, heating at 130°C for28 h, cooling to room temp.; pouring into CH2Cl2, filtration through silica pad, washing with CH2Cl2,concn. in vac., distillation of diisopropylbenzene in vac., crystn. (et her, 0°C); elem. anal.;
参考文献
Lokare, Kapil S.; Staples, Richard J.; Odom, Aaron L.
Organometallics, 2008 , vol. 27, # 19 p. 5130 - 5138
