5-溴-2-甲氧基苯甲醛合成路线 （共 49 条）
反应条件
in benzene 2 h; Heating;
参考文献
Trivedi, G. S.; Desai, N. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 6 p. 366 - 369
反应条件
sulfuric acid; nitric acid T=-15°C; 2 h;
参考文献
TORAY INDUSTRIES, INC.
Patent: US2012/184735 A1, 2012 ;
Location in patent: Page/Page column 25 ;
反应条件
1: 95 percent / dimethylformamide / 12 h / Ambient temperature 2: 94 percent / conc. H2SO4 / 2 h / Ambient temperature View Scheme
参考文献
Armstrong, Veronica; Soto, Oriana; Valderrama, Jaime A.; Tapia, Ricardo
Synthetic Communications, 1988 , vol. 18, # 7 p. 717 - 726
参考文献
Tang, Jing; Huang, Xian
Journal of Chemical Research - Part S, 2003 , # 6 p. 354 - 355
反应条件
1: CH3ONa / methanol / 5 h / 0 °C 2: xylene / 3 h / Heating 3: 96 percent / aq. KOH / 2 h / Heating 4: 77 percent / chromite de cuivre (active par du baryum) / quinoline / 7 h / 190 °C View Scheme
参考文献
Kim, Phieo Ta; Guillard, Roger; Samreth, Soth; Sornay, Roland
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 1373 - 1377
反应条件
sodium tetrahydroborate in tetrahydrofuran; water
参考文献
Sankyo Co., Ltd.
Patent: JP2005/120047 A, 2005 ;
Location in patent: Page/Page column 89-90 ;
反应条件
1: LiAlH4 / tetrahydrofuran / 20 h / Heating 2: pyridine, thionyl chloride / toluene / 24 h / Ambient temperature 3: KI / dimethylsulfoxide / 20 h / Ambient temperature View Scheme
参考文献
Langlois, Michel; Bremont, Beatrice; Shen, Shuren; Poncet, Annie; Andrieux, Jean; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 12 p. 2050 - 2060
反应条件
1: 1.) 30percent peracetic acid; 2.) FeSO4 / 1.) acetic acid, room temp., 16 h; 2.) H2O, 20 min 2: 85 percent / NaOH / H2O / 1.) room temp., 1 h; 2.) reflux, 40 min View Scheme
参考文献
Tercio, J.; Ferreira, B.; Catani, V.; Comasseto, J. V.
Synthesis, 1987 , # 2 p. 149 - 153
反应条件
toluene-4-sulfonic acid in toluene Heating;
参考文献
Hall, C. Dennis; Sachsinger, Niki; Nyburg, Stanley C.; Steed, Jonathan W.
Journal of Organometallic Chemistry, 1998 , vol. 561, # 1-2 p. 209 - 219
反应条件
toluene-4-sulfonic acid in ethylene glycol; toluene
参考文献
Pfizer Inc.
Patent: US5837711 A1, 1998 ;
