1,3-双(2,6-二异丙基苯基)氯化咪唑鎓合成路线 (共 13 条)
反应条件
chloro-trimethyl-silane in ethyl acetate T=70°C; 2.75 h; Inert atmosphere;
参考文献
Tang, Pingping; Wang, Weike; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 30 p. 11482 - 11484
反应条件
in tetrahydrofuran T=20°C; 24 h; Molecular sieveInert atmosphere;
参考文献
Higgins, Eleanor M.; Sherwood, Jennifer A.; Lindsay, Anita G.; Armstrong, James; Massey, Richard S.; Alder, Roger W.; O'Donoghue, Annmarie C.
Chemical Communications, 2011 , vol. 47, # 5 p. 1559 - 1561
反应条件
trichlorosilane in toluene T=25°C; 12 h; Inert atmosphere;
参考文献
Ghadwal, Rajendra S.; Roesky, Herbert W.; Merkel, Sebastian; Henn, Julian; Stalke, Dietmar
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 5683 - 5686
Angewandte Chemie, 2009 , vol. 121, p. 5793 - 5796
反应条件
trifluoroacetic acid in chloroform-d1 T=20°C; 12 h; Inert atmosphere;
参考文献
Fu, Ching-Feng; Lee, Chun-Chin; Liu, Yi-Hung; Peng, Shie-Ming; Warsink, Stefan; Elsevier, Cornelis J.; Chen, Jwu-Ting; Liu, Shiuh-Tzung
Inorganic Chemistry, 2010 , vol. 49, # 6 p. 3011 - 3018
反应条件
hydrogenchloride in methanol 36 h; Reflux;
参考文献
Huerta-Aguilar, Carlos; Talamantes Gomez, Jose M.; Thangarasu, Pandiyan; Camacho-Arroyo, Ignacio; Gonzalez-Arenas, Aliesha; Narayanan, Jayanthi; Srivastava, Rajendra
Applied Organometallic Chemistry, 2013 , vol. 27, # 10 p. 578 - 587
反应条件
1.1: 77.5 percent / formic acid / ethanol; H2O / 48 h 2.1: toluene / 100 °C 2.2: 47 percent / HCl / toluene; dioxane / 5 h / 70 °C View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 606, # 1 p. 49 - 54
反应条件
T=-30 - 20°C; 50 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 52 p. 14204 - 14208
Angew. Chem., , vol. 125, # 52 p. 14454 - 14458,5
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 16 p. 2929 - 2932
反应条件
sodium t-butanolate in tetrahydrofuran T=20°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Wu, Shaoxiang; Guo, Jiyi; Sohail, Muhammad; Cao, Chengyao; Chen, Fu-Xue
Journal of Fluorine Chemistry, 2013 , vol. 148, p. 19 - 29
反应条件
in tetrahydrofuran T=20°C;
参考文献
Knappke, Christiane E. I.; Arduengo, Anthony J.; Jiao, Haijun; Neudoerfl, Joerg-Martin; Jacobivonwangelin, Axel
Synthesis, 2011 , # 23 art. no. T79311SS, p. 3784 - 3795