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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5’-氨基磺酰基腺苷
合成路线
（共 7 条）
863238-53-3
→
反应条件
25030-31-3
5’-氨基磺酰基腺苷
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 0.5 h;
参考文献
SLOAN-KETTERING INSTITUTE FOR CANCER RESEARCH; CORNELL RESEARCH FOUNDATION, INC.
Patent: WO2006/113615 A2, 2006 ;
Location in patent: Page/Page column 90-91; 7/23 ;
1356085-21-6
→
反应条件
25030-31-3
5’-氨基磺酰基腺苷
+
713543-21-6
反应条件
palladium 10 on activated carbon; hydrogen in water; isopropyl alcohol T=70°C; P=37503.8 Torr; 2 h; Continuous-flow hydrogenation reactor;
参考文献
Redwan, Itedale Namro; Ljungdahl, Thomas; Grotli, Morten
Tetrahedron, 2012 , vol. 68, # 5 p. 1507 - 1514
1356085-30-7
→
反应条件
25030-31-3
5’-氨基磺酰基腺苷
反应条件
palladium 10 on activated carbon; hydrogen in water; isopropyl alcohol T=70°C; P=37503.8 Torr; 2 h; Continuous-flow hydrogenation reactor;
参考文献
Redwan, Itedale Namro; Ljungdahl, Thomas; Grotli, Morten
Tetrahedron, 2012 , vol. 68, # 5 p. 1507 - 1514
112921-00-3
→
反应条件
25030-31-3
5’-氨基磺酰基腺苷
反应条件
1: With water; trifluoroacetic acid T=20°C; 1 h; 2: With ammonium hydroxide in methanol; dichloromethane
参考文献
Lukkarila, Julie L.; Da Silva, Sara R.; Ali, Mohsin; Shahani, Vijay M.; Xu, G. Wei; Berman, Judd; Roughton, Andrew; Dhe-Paganon, Sirano; Schimmer, Aaron D.; Gunning, Patrick T.
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 8 p. 577 - 582
64-17-5
乙醇
→
反应条件
25030-31-3
5’-氨基磺酰基腺苷
反应条件
palladium 10 on activated carbon; hydrogen in water T=50°C; P=37503.8 Torr; 1.33333 h; Continuous-flow hydrogenation reactor;
参考文献
Redwan, Itedale Namro; Ljungdahl, Thomas; Grotli, Morten
Tetrahedron, 2012 , vol. 68, # 5 p. 1507 - 1514
362-75-4
2',3'-异丙叉腺苷
→
反应条件
25030-31-3
5’-氨基磺酰基腺苷
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.5 h / Inert atmosphere; Cooling with ice 1.2: 2 h / 20 °C / Inert atmosphere; Cooling with ice 2.1: water; trifluoroacetic acid / 1 h / 20 °C View Scheme
参考文献
Lukkarila, Julie L.; Da Silva, Sara R.; Ali, Mohsin; Shahani, Vijay M.; Xu, G. Wei; Berman, Judd; Roughton, Andrew; Dhe-Paganon, Sirano; Schimmer, Aaron D.; Gunning, Patrick T.
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 8 p. 577 - 582
58-61-7
腺苷
→
反应条件
25030-31-3
5’-氨基磺酰基腺苷
反应条件
1.1: toluene-4-sulfonic acid / 3 h / 20 °C 2.1: sodium hydride / tetrahydrofuran / 0.5 h / Inert atmosphere; Cooling with ice 2.2: 2 h / 20 °C / Inert atmosphere; Cooling with ice 3.1: water; trifluoroacetic acid / 1 h / 20 °C View Scheme
参考文献
Lukkarila, Julie L.; Da Silva, Sara R.; Ali, Mohsin; Shahani, Vijay M.; Xu, G. Wei; Berman, Judd; Roughton, Andrew; Dhe-Paganon, Sirano; Schimmer, Aaron D.; Gunning, Patrick T.
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 8 p. 577 - 582
