9,9-二己基芴-2,7-二硼酸二(1,3-丙二醇)酯合成路线 (共 6 条)
参考文献
Ling; Kang; Neoh; Huang, Wei
Macromolecules, 2003 , vol. 36, # 19 p. 6995 - 7003
反应条件
1.1: Mg / tetrahydrofuran 1.2: tetrahydrofuran / -78 - 20 °C 2.1: toluene / Heating View Scheme
参考文献
Macromolecules, , vol. 37, # 19 p. 7078 - 7080
反应条件
1.1: 96 percent / triethylbenzylammonium chloride; aq. NaOH / dimethylsulfoxide 2.1: Mg; I2 / tetrahydrofuran / Heating 2.2: tetrahydrofuran / -78 °C 3.1: aq. H2SO4 4.1: 88 percent / toluene / Heating View Scheme
参考文献
Macromolecules, , vol. 36, # 19 p. 6995 - 7003
反应条件
1.1: NaOH; H2O; TBACl / 80 °C 2.1: Mg / tetrahydrofuran 2.2: B(OMe)3 / tetrahydrofuran / 50 h / -78 - 20 °C 2.3: 60 percent / H2SO4; H2O 3.1: toluene / 3 h / Heating View Scheme
参考文献
Chemical Communications, , # 18 p. 1837 - 1838
参考文献
Macromolecules, , vol. 37, # 19 p. 7078 - 7080
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran; water
Suzuki coupling; 48 h; Inert atmosphereReflux;
参考文献
Yamaguchi, Isao; Seo, Kenji; Kawashima, Yukari
Tetrahedron, 2010 , vol. 66, # 34 p. 6725 - 6732