1-甲基-2,3,4,9-四氢-1H-吡啶并[3,4-b]吲哚合成路线 （共 6 条）
反应条件
C21H21ClIrNO2 in tetrahydrofuran; 2,2,2-trifluoroethanol 20 h; Inert atmosphere;
参考文献
Wu, Jianjun; Talwar, Dinesh; Johnston, Steven; Yan, Ming; Xiao, Jianliang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., 2013 , vol. 125, # 27 p. 7121 - 7125,5
反应条件
1: cis-maleic acid; palladium on activated charcoal / water / 8 h / |Reflux 2: sodium nitrate; trifluoroacetic acid / 6 h / 0 - 20 °C View Scheme
参考文献
Song, Hongjian; Liu, Yongxian; Liu, Yuxiu; Wang, Lizhong; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 5 p. 1010 - 1018
反应条件
1: cis-maleic acid; palladium on activated charcoal / water / 8 h / |Reflux
2: N-bromosuccinmide / acetic acid / 6 h / 20 °C
View Scheme
参考文献
Song, Hongjian; Liu, Yongxian; Liu, Yuxiu; Wang, Lizhong; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 5 p. 1010 - 1018
反应条件
1: cis-maleic acid; palladium on activated charcoal / water / 8 h / |Reflux
2: sodium nitrate; trifluoroacetic acid / 6 h / 0 - 20 °C
View Scheme
参考文献
Song, Hongjian; Liu, Yongxian; Liu, Yuxiu; Wang, Lizhong; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 5 p. 1010 - 1018
反应条件
hydrogenchloride; borane-ammonia complex in aq. phosphate buffer; N,N-dimethyl-formamide
T=37°C; pH=7.8; 24 h;
参考文献
Ghislieri, Diego; Green, Anthony P.; Pontini, Marta; Willies, Simon C.; Rowles, Ian; Frank, Annika; Grogan, Gideon; Turner, Nicholas J.
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10863 - 10869
反应条件
hydrogenchloride; sodium nitrite in ethanol
T=37°C; pH=3; 1 h;
参考文献
Diem, Stefanie; Gutsche, Birgit; Herderich, Markus
Journal of Agricultural and Food Chemistry, 2001 , vol. 49, # 12 p. 5993 - 5998
