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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-Cbz-吡咯烷
合成路线
（共 32 条）
25070-74-0
1-Cbz-吡咯烷
→
反应条件
5105-78-2
N-苄氧羰基-4-氨基丁酸
反应条件
ruthenium(IV) oxide; sodium periodate in tert-butyl alcohol T=20°C; 3 h;
参考文献
Kaname, Mamoru; Yoshifuji, Shigeyuki; Sashida, Haruki
Tetrahedron Letters, 2008 , vol. 49, # 17 p. 2786 - 2788
25070-74-0
1-Cbz-吡咯烷
→
反应条件
100858-32-0
(S)-(+)-1-Cbz-3-吡咯烷醇
+
100858-33-1
N-CBZ-3-(R)-羟基吡咯烷
反应条件
D-glucose; Reduced nicotinamide-adenine dinucleotide in methanol; water T=25°C; pH=8; 0.25 h; aq. potassium phosphate bufferEnzymatic reaction; Kinetics; ConcentrationReagent/catalyst; optical yield given as percent eeenantioselective reaction;
参考文献
Zhang, Wei; Tang, Weng Lin; Wang, Zunsheng; Li, Zhi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3380 - 3390
25070-74-0
1-Cbz-吡咯烷
→
反应条件
100858-33-1
N-CBZ-3-(R)-羟基吡咯烷
反应条件
D-glucose; Sphingomonas sp. HXN-200 in phosphate buffer T=30°C; pH=7.5; 0.5 h; Enzymatic reaction;
参考文献
Li; Feiten; Chang; Duetz; Van Beilen; Witholt
Journal of Organic Chemistry, 2001 , vol. 66, # 25 p. 8424 - 8430
25070-74-0
1-Cbz-吡咯烷
→
反应条件
100858-32-0
(S)-(+)-1-Cbz-3-吡咯烷醇
+
100858-33-1
N-CBZ-3-(R)-羟基吡咯烷
反应条件
D-glucose; Reduced nicotinamide-adenine dinucleotide in methanol; water T=25°C; pH=8; 0.25 h; aq. potassium phosphate bufferEnzymatic reaction; Kinetics; ConcentrationReagent/catalyst; optical yield given as percent eeenantioselective reaction;
参考文献
Zhang, Wei; Tang, Weng Lin; Wang, Zunsheng; Li, Zhi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3380 - 3390
123-75-1
四氢吡咯
+
501-53-1
氯甲酸苄酯
→
反应条件
25070-74-0
1-Cbz-吡咯烷
反应条件
sodium hydroxide in water T=0 - 20°C;
参考文献
Myers, Eddie L.; De Vries, Johannes G.; Aggarwal, Varinder K.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 11 p. 1893 - 1896
88001-42-7
→
反应条件
25070-74-0
1-Cbz-吡咯烷
反应条件
N,N-diethyl-N-isopropylamine; trifluoroacetic acid trimethylsilyl ester in dichloromethane; pentane T=0°C; 0.583333 h;
参考文献
BRISTOL-MYERS SQUIBB COMPANY
Patent: WO2005/12249 A2, 2005 ;
Location in patent: Page/Page column 40 ;
WO 2005/012249 A2
→
反应条件
1203491-06-8
+
25070-74-0
1-Cbz-吡咯烷
反应条件
samarium diiodide; boron trifluoride diethyl etherate; tert-butyl alcohol in tetrahydrofuran T=-40°C;
参考文献
Xiang, Yong-Gang; Wang, Xiang-Wu; Zheng, Xiao; Ruan, Yuan-Ping; Huang, Pei-Qiang
Chemical Communications, 2009 , # 45 p. 7045 - 7047
1663-39-4
丙烯酸叔丁酯
→
反应条件
反应条件
bis(cyclopentadienyl)titanium dichloride; chloro-trimethyl-silane; magnesium; tert-butyl alcohol in tetrahydrofuran T=20°C; Inert atmosphere; Reagent/catalyst;
参考文献
Zheng, Xiao; Dai, Xi-Jie; Yuan, Hong-Qiu; Ye, Chen-Xi; Ma, Jie; Huang, Pei-Qiang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 12 p. 3494 - 3498
Angew. Chem., 2013 , vol. 125, # 12 p. 3578 - 3582,5
→
反应条件
反应条件
bis(cyclopentadienyl)titanium dichloride; chloro-trimethyl-silane; magnesium; tert-butyl alcohol in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Zheng, Xiao; Dai, Xi-Jie; Yuan, Hong-Qiu; Ye, Chen-Xi; Ma, Jie; Huang, Pei-Qiang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 12 p. 3494 - 3498
Angew. Chem., 2013 , vol. 125, # 12 p. 3578 - 3582,5
1629-58-9
1-戊烯-3-酮
→
反应条件
25070-74-0
1-Cbz-吡咯烷
反应条件
bis(cyclopentadienyl)titanium dichloride; chloro-trimethyl-silane; magnesium; tert-butyl alcohol in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Zheng, Xiao; Dai, Xi-Jie; Yuan, Hong-Qiu; Ye, Chen-Xi; Ma, Jie; Huang, Pei-Qiang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 12 p. 3494 - 3498
Angew. Chem., 2013 , vol. 125, # 12 p. 3578 - 3582,5
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