sodium tetrahydroborate in tetrahydrofuran; ethanol T=5°C; 1 h; Inert atmosphere;
参考文献
Grainger, Richard S.; Patel, Bhaven; Kariuki, Benson M.; Male, Louise; Spencer, Neil
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 5843 - 5852
1.1: n-butyllithium / diethyl ether; hexane / 1.17 h / -20 - 10 °C / Inert atmosphere 1.2: 3 h / Inert atmosphere; Reflux 1.3: -78 - 20 °C / Inert atmosphere 2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 1 h / 5 °C / Inert atmosphere View Scheme
参考文献
Grainger, Richard S.; Patel, Bhaven; Kariuki, Benson M.; Male, Louise; Spencer, Neil
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 5843 - 5852