3-甲基-3-苯基丁酸甲酯合成路线 （共 12 条）
参考文献
Saboor
Journal of the Chemical Society, 1945 , p. 922,924
参考文献
Yakugaku Zasshi, , vol. 76, p. 163,165, 166
Chem.Abstr., , p. 13850
反应条件
1: 3-Methyl-3-phenyl-butanoic acid With caesium carbonate in tetrahydrofuran; N,N-dimethyl-formamide
Heating / reflux;
2: methyl iodide in tetrahydrofuran; N,N-dimethyl-formamide
15 h; Heating / reflux;
参考文献
MERCK and CO., INC.
Patent: WO2007/108968 A2, 2007 ;
Location in patent: Page/Page column 30 ;
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 2-chloro-1,2-diphenyl-ethanone
T=60°C;
参考文献
Zhao, Yingsheng; Jin, Liqun; Li, Peng; Lei, Aiwen
Journal of the American Chemical Society, 2008 , vol. 130, # 29 p. 9429 - 9433
反应条件
thionyl chloride
Erwaermen des Reaktionsprodukts mit Benzol und Aluminiumchlorid;
参考文献
Saboor
Journal of the Chemical Society, 1945 , p. 922,924
反应条件
1: aluminum chloride
2: thionyl chloride
View Scheme
参考文献
Liehr, Joachim G.; Caprioli, Richard M.; Beynon, John H.; Morgan, Roger P.; Richter, Wilhelm J.
Organic Mass Spectrometry, 1980 , vol. 15, # 3 p. 157 - 160
反应条件
1: aluminum chloride
2: thionyl chloride
View Scheme
参考文献
Liehr, Joachim G.; Caprioli, Richard M.; Beynon, John H.; Morgan, Roger P.; Richter, Wilhelm J.
Organic Mass Spectrometry, 1980 , vol. 15, # 3 p. 157 - 160
反应条件
1: AlCl3 / anschliessenden Kochen mit absol. Methanol
2: thionyl chloride / Erwaermen des Reaktionsprodukts mit Benzol und Aluminiumchlorid
View Scheme
参考文献
Saboor
Journal of the Chemical Society, 1945 , p. 922,924
参考文献
Liehr, Joachim G.; Caprioli, Richard M.; Beynon, John H.; Morgan, Roger P.; Richter, Wilhelm J.
Organic Mass Spectrometry, 1980 , vol. 15, # 3 p. 157 - 160
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran
7 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brueckner, Christiane; Reissig, Hans-Ulrich
Chemische Berichte, 1987 , vol. 120, p. 627 - 630
