噻吩并[3,2-b]噻吩合成路线 (共 55 条)
反应条件
quinoline; copper T=260°C; 0.5 h;
参考文献
Fuller, Lance S.; Iddon, Brian; Smith, Kevin A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3465 - 3470
反应条件
gold(I) chloride in 1,4-dioxane; water T=20°C; 3 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Katsuta, Hiroshi; Toyota, Kozo; Iwamoto, Takeaki; Morita, Noboru
Bulletin of the Chemical Society of Japan, 2012 , vol. 85, # 5 p. 613 - 623
反应条件
1: 81 percent / K2CO3 / dimethylformamide / 72 h / Ambient temperature 2: 90 percent / aq. LiOH / tetrahydrofuran / 3 h / Heating 3: 88 percent / Cu, quinoline / 0.5 h / 260 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 22 p. 3465 - 3470
反应条件
phosphorus pentoxide; benzene
参考文献
Proceedings - Indian Academy of Sciences, Section A, , # 39 p. 14,17
反应条件
1: 90 percent / aq. LiOH / tetrahydrofuran / 3 h / Heating 2: 88 percent / Cu, quinoline / 0.5 h / 260 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 22 p. 3465 - 3470
反应条件
in toluene T=110°C; 0.833333 h;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 74, # 5 p. 785 - 798
反应条件
1: SOCl2 / diethyl ether / 4 h / Heating 2: 1.80 g / AlCl3 / 1,2-dichloro-ethane / 18 h / Heating 3: NaBH4 / methanol; CH2Cl2 / 3 h / 20 °C 4: 0.30 g / aq. HCl / methanol; CH2Cl2 / 0.5 h / 20 °C View Scheme
参考文献
Journal of Materials Chemistry, , vol. 13, # 6 p. 1324 - 1332
参考文献
Archer, William J.; Roger, Taylor
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 295 - 300
反应条件
1: 1.) 5percent methanolic KOH, (E)-3-acetylthio-2-(2-acetylthiovinyl)thiophene, 2.) I2 / 1.) ambient temp., 1 h, 2.) MeOH, 30 min 2: dimethylsulfoxide-d6 / 2 h / Irradiation View Scheme
参考文献
Tetrahedron, , vol. 53, # 22 p. 7509 - 7528
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; water
参考文献
Heterocycles, , vol. 45, # 10 p. 1891 - 1894