3,5-二叔丁基-4-羟基苯甲酸甲酯合成路线 （共 24 条）
反应条件
thionyl chloride; triethylamine in N-methyl-acetamide; methanol; dichloromethane
参考文献
The Green Cross Corporation
Patent: US5750545 A1, 1998 ;
反应条件
sodium hydroxide; potassium hexacyanoferrate(III) in benzene 1 h;
参考文献
Pugovics, Osvalds; Kauss, Valerjans; Kalvinsh, Ivars; Gold, Markus R.
Journal of Chemical Research - Part S, 1998 , # 8 p. 470 - 471
反应条件
C5CoN5O2(3-)*3C36H30NP2(1+) in dichloromethane T=-70°C; 0.166667 h; starting material added in dimer form;
参考文献
Tetrahedron Letters, , vol. 21, p. 3407 - 3408
反应条件
hydrogenchloride 10 h; Heating;
参考文献
Pastor, Stephen D.; Hessell, Edward T.
Journal of Organometallic Chemistry, 1987 , vol. 328, p. 263 - 274
反应条件
sodium methylate in methanol Ambient temperatureelectrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.5 V; 0.1 M NaClO4;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 33, # 9 p. 4007 - 4011
参考文献
Justus Liebigs Annalen der Chemie, , vol. 645, p. 36 - 52
反应条件
1: 1.) t-BuLi / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C to rt 2: aq. HCl / diethyl ether / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 25 p. 9462 - 9469
反应条件
hydrogenchloride in diethyl ether Heating; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 25 p. 9462 - 9469
反应条件
1: 61 percent / sodium methoxide / diethyl ether / 25 °C / electrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.12 V; 0.1 M NaClO4 2: 41 percent / sodium methoxide / methanol / Ambient temperature; electrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.5 V; 0.1 M NaClO4 View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 33, # 9 p. 4007 - 4011
反应条件
1: NH2OH*HCl, Py / ethanol; methanol / Heating 2: H2SO4 / Heating View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 645, p. 36 - 52
