2,3,5-三溴噻吩并[3,2-b]噻吩合成路线 （共 6 条）
反应条件
bromine in chloroform T=0 - 20°C;
参考文献
Archer, William J.; Taylor, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 301 - 306
反应条件
water; bromine; acetic acid 1.) r.t., 1 h, 2.) reflux; Yield given. Multistep reaction;
参考文献
Fuller, Lance S.; Iddon, Brian; Smith, Kevin A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3465 - 3470
反应条件
1: 78 percent / LDA, Br2 / tetrahydrofuran; hexane / 1.) -80 deg C, 5 min, 2.) -80 deg C to r.t. 2: 76 percent / Zn, AcOH / 1 h / Heating View Scheme
参考文献
Fuller, Lance S.; Iddon, Brian; Smith, Kevin A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3465 - 3470
反应条件
bromine; lithium diisopropyl amide in tetrahydrofuran; hexane 1.) -80 deg C, 5 min, 2.) -80 deg C to r.t.;
参考文献
Fuller, Lance S.; Iddon, Brian; Smith, Kevin A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3465 - 3470
反应条件
zinc in acetic acid 10 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 7 p. 2165 - 2173
反应条件
zinc in acetic acid 10 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 7 p. 2165 - 2173
