反应条件
1.1: PhBCl2 / 1,2-dichloro-ethane / 1 h / 0 °C
1.2: 32 percent / iPr2NEt / 1,2-dichloro-ethane / 4.5 h / 0 - 20 °C
2.1: 16 percent / various solvent(s) / 2.5 h / 180 °C
3.1: 51 percent / TFA; (PPh3)4RhH / ethanol / 1.75 h / 85 °C
View Scheme
参考文献
Zakrzewski, Peter; Gowan, Mathew; Trimble, Laird A.; Lau, Cheuk K.
Synthesis, 1999 , # 11 p. 1893 - 1902
