2-(2-氯苯氧基)丙酸合成路线 (共 12 条)
反应条件
phosphate buffer; β-cyclodextrin T=37°C; 2 h; bovine serum albumin (BSA); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 2, # 1 p. 39 - 42
反应条件
L-leuconol-derived ionic liquid in phosphate buffer T=20°C; pH=7.5;
参考文献
Analytical Chemistry, , vol. 78, # 19 p. 7061 - 7069
反应条件
1: p-toluenesulfonic acid, 2,2-dimethoxypropane / 4 h / 55 °C 2: phosphate buffer, pH 7.00 / α-chimotripsine / H2O / 42 h / 20 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 66, p. 1219 - 1222
反应条件
Candida cylindracea lipase in water; dimethyl sulfoxide T=30°C; 1.1 h; 0.1 M pH 7.5 phosphate buffer; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 28, # 40 p. 4661 - 4664
反应条件
water in tert-butyl methyl ether T=35°C; 1 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Chirality, , vol. 24, # 1 p. 60 - 66
反应条件
Birman's catalyst; trimethylacetic anhydride; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C; 24 h; Inert atmosphere; enantioselective reaction;
参考文献
Heterocycles, , vol. 86, # 2 p. 1227 - 1252
反应条件
2: Candida cylindracea lipase / H2O; dimethylsulfoxide / 1.1 h / 30 °C / 0.1 M pH 7.5 phosphate buffer View Scheme
参考文献
Tetrahedron Letters, , vol. 28, # 40 p. 4661 - 4664
反应条件
phosphate buffer; β-cyclodextrin T=37°C; 2 h; bovine serum albumin (BSA); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 2, # 1 p. 39 - 42
反应条件
phosphate buffer; β-cyclodextrin T=37°C; 3 h; bovine serum albumin (BSA); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 2, # 1 p. 39 - 42
反应条件
phosphate buffer; C. cylindracea lipase; [14C]-Dextromethorphan T=24°C; 7 h; other amines, other times, enetioselectivity of hydrolysis, other ojects of study; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 17 p. 6836 - 6841