9-甲基-10-(氯甲基)蒽合成路线 (共 8 条)
反应条件
hydrogenchloride in acetic acid 1 h;
参考文献
Bodoev, N.V.; Krysin, A.P.; Koptyug, V.A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 880 - 885
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 5 p. 1002 - 1008
反应条件
hydrogenchloride; acetic acid anschliessend mit 9-Methyl-anthracen;
参考文献
Badger; Pearce
Journal of the Chemical Society, 1950 , p. 2314,2316
反应条件
1: tetrahydrofuran / 20 °C 2: 8 percent / LAH / tetrahydrofuran / 70 °C View Scheme
参考文献
Takagi, Masato; Hirabe, Tomoatsu; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1311 - 1314
反应条件
1: NaOH / aq. ethanol; methanol 2: SOCl2 / dioxane View Scheme
参考文献
Peck; O'Connell; Creech
Journal of medicinal chemistry, 1967 , vol. 10, # 1 p. 37 - 40
反应条件
methyl-magnesium iodide
参考文献
Stewart,F.H.C.
Australian Journal of Chemistry, 1961 , vol. 14, p. 177 - 181
反应条件
1: tetrahydrofuran / 20 °C
2: LAH / tetrahydrofuran / 70 °C
View Scheme
参考文献
Takagi, Masato; Hirabe, Tomoatsu; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1311 - 1314
反应条件
1: tetrahydrofuran / 20 °C
2: LAH / diethyl ether / 5 h / Heating
View Scheme
参考文献
Takagi, Masato; Hirabe, Tomoatsu; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1311 - 1314
反应条件
methyl-magnesium iodide
参考文献
Stewart,F.H.C.
Australian Journal of Chemistry, 1961 , vol. 14, p. 177 - 181