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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴苯并噻唑
合成路线
（共 25 条）
2516-40-7
2-溴苯并噻唑
+
214360-73-3
4-氨基苯硼酸频哪醇酯
→
反应条件
6278-73-5
4-(2-苯并噻唑基)苯胺
反应条件
potassium carbonate; tris(dibenzylideneacetone)dipalladium (0) in ethylene glycol dimethyl ether; water T=100°C; Suzuki biaryl coupling; 6 h;
参考文献
Majo, Vattoly J.; Prabhakaran, Jaya; Mann, J. John; Kumar, J. S. Dileep
Tetrahedron Letters, 2003 , vol. 44, # 47 p. 8535 - 8537
2516-40-7
2-溴苯并噻唑
+
1679-18-1
4-氯苯硼酸
→
反应条件
6265-91-4
2-(4-氯苯基)苯并噻唑
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethylene glycol dimethyl ether; water T=150°C; Suzuki coupling; Microwave irradiationCombinatorial reaction / High throughput screening (HTS);
参考文献
Auld, Douglas S.; Zhang, Ya-Qin; Southall, Noel T.; Rai, Ganesha; Landsman, Marc; MacLure, Jennifer; Langevin, Daniel; Thomas, Craig J.; Austin, Christopher P.; Inglese, James
Journal of Medicinal Chemistry, 2009 , vol. 52, # 5 p. 1450 - 1458
2516-40-7
2-溴苯并噻唑
→
反应条件
136-95-8
2-氨基苯并噻唑
反应条件
ammonium hydroxide; potassium phosphate; 1-(5,6,7,8-tetrahydroquinolin-8-yl)-2-methylpropan-1-one; copper(I) bromide in dimethyl sulfoxide T=110°C; 24 h; Inert atmosphereSealed tube;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 11-12 p. 1722 - 1726
2516-40-7
2-溴苯并噻唑
→
反应条件
1123-98-4
2-氟苯并噻唑
反应条件
potassium fluoride; 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane in dimethyl sulfoxide T=150°C; 0.166667 h; Microwave irradiation;
参考文献
Simeon, Fabrice G.; Wendahl, Matthew T.; Pike, Victor W.
Tetrahedron Letters, 2010 , vol. 51, # 46 p. 6034 - 6036
2516-40-7
2-溴苯并噻唑
+
768-35-4
3-氟苯基硼酸
→
反应条件
1629-07-8
2-(3-氟苯基)-1,3-苯并噻唑
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethylene glycol dimethyl ether; water T=150°C; Suzuki coupling; Microwave irradiationCombinatorial reaction / High throughput screening (HTS);
参考文献
Auld, Douglas S.; Zhang, Ya-Qin; Southall, Noel T.; Rai, Ganesha; Landsman, Marc; MacLure, Jennifer; Langevin, Daniel; Thomas, Craig J.; Austin, Christopher P.; Inglese, James
Journal of Medicinal Chemistry, 2009 , vol. 52, # 5 p. 1450 - 1458
2516-40-7
2-溴苯并噻唑
+
28611-39-4
4-二甲基氨基苯硼酸
→
反应条件
10205-56-8
(4-苯并噻唑-2-基-苯基)-二甲基-胺
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethylene glycol dimethyl ether; water T=150°C; Suzuki coupling; Microwave irradiationCombinatorial reaction / High throughput screening (HTS);
参考文献
Auld, Douglas S.; Zhang, Ya-Qin; Southall, Noel T.; Rai, Ganesha; Landsman, Marc; MacLure, Jennifer; Langevin, Daniel; Thomas, Craig J.; Austin, Christopher P.; Inglese, James
Journal of Medicinal Chemistry, 2009 , vol. 52, # 5 p. 1450 - 1458
2516-40-7
2-溴苯并噻唑
+
74497-02-2
→
反应条件
1843-21-6
N-苯基-1,3-苯并噻唑-2-胺
反应条件
copper(l) iodide; potassium carbonate in dimethyl sulfoxide T=120°C; 48 h; Green chemistry;
参考文献
Toulot, Stephanie; Heinrich, Timo; Leroux, Frederic R.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 16 p. 3263 - 3272
2516-40-7
2-溴苯并噻唑
+
1765-93-1
4-氟苯硼酸
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
potassium carbonate; tris(dibenzylideneacetone)dipalladium (0) in ethylene glycol dimethyl ether; water T=100°C; Suzuki biaryl coupling; 6 h;
参考文献
Majo, Vattoly J.; Prabhakaran, Jaya; Mann, J. John; Kumar, J. S. Dileep
Tetrahedron Letters, 2003 , vol. 44, # 47 p. 8535 - 8537
2516-40-7
2-溴苯并噻唑
+
20277-69-4
甲烷亚磺酸钠
→
反应条件
934-34-9
2-羟基苯并噻唑
+
7144-49-2
2-(甲磺酰基)苯并噻唑
反应条件
in dimethyl sulfoxide T=110°C; 10 h; Overall yield = 47.5 mg;
参考文献
Liang, Shuai; Zhang, Ruo-Yi; Xi, Long-Yi; Chen, Shan-Yong; Yu, Xiao-Qi
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 11874 - 11880
2516-40-7
2-溴苯并噻唑
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
321547-37-9
+
22779-05-1
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in N,N-dimethyl-formamide T=20°C; Sonogashira Cross-Coupling; 4 h; Inert atmosphereSchlenk technique; Catalytic behavior;
参考文献
Lu, Linhua; Yan, Hong; Sun, Peng; Zhu, Yan; Yang, Hailong; Liu, Defu; Rong, Guangwei; Mao, Jincheng
European Journal of Organic Chemistry, 2013 , # 9 p. 1644 - 1648
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