1: KOH / methanol / 1.) room temperature, 14 h, 2.) reflux, 1 h
2: NCS / CCl4 / 14 h / Ambient temperature
3: TFA / 1 h / -6 °C
4: NaIO4 / methanol; H2O / Ambient temperature
5: 0.5 h / 130 °C / 20 Torr
View Scheme
参考文献
Harvey, Jeremy; Brichard, Marie-Helene; Viehe, Heinz G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 19 p. 2275 - 2280