1,1,2,2-四甲氧基乙烷合成路线 （共 16 条）
反应条件
zirconium sulphate 2 h; Heating;
参考文献
Degussa AG
Patent: EP1460052 A1, 2004 ;
Location in patent: Page 4; 5 ;
反应条件
zirconium sulphate; magnesium sulfate in chloroform; water 24 h; Heating;
参考文献
Sangsari, Farid Hamedi; Chastrette, Francine; Chastrette, Maurice
Synthetic Communications, 1988 , vol. 18, # 12 p. 1343 - 1348
反应条件
toluene-4-sulfonic acid in water Heating / reflux;
参考文献
Degussa AG
Patent: EP1460052 A1, 2004 ;
Location in patent: Page 5 ;
参考文献
Heydrich, Gunnar; Aust, Nicola Christiane; Putter, Hermann; Fischer, Andreas; Botzem, Jorg
Patent: US2003/69451 A1, 2003 ;
参考文献
DEGUSSA AG
Patent: US2004/186304 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
chlorine anschliessend Behandeln mit Methanol;
参考文献
Schreyer
Journal of the American Chemical Society, 1951 , vol. 73, p. 2962
反应条件
LEWATIT.(R). K2629 in water T=65°C;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2005/23743 A1, 2005 ;
Location in patent: Page/Page column 17-23, chart 1/2; 2/2 ;
参考文献
Fischer; Taube
Chemische Berichte, 1926 , vol. 59, p. 854
反应条件
thionyl chloride; phosphorus pentachloride 1.) CCl4, 0-25 deg C, 6 h; 2.) room temp., overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bou, Anna; Pericas,Miquel A.; Serratosa, Felix
Tetrahedron, 1981 , vol. 37, p. 1441 - 1449
参考文献
Fiesselmann; Hoerndler
Chemische Berichte, 1954 , vol. 87, p. 906,910
