2-(3-氧代-2,3-二氢-1H-茚-1-基)乙酸合成路线 （共 13 条）
反应条件
1: With thionyl chloride
0.5 h; Heating / reflux;
2: With AlCl3, aluminium chloride in nitrobenzene
T=80°C; Friedel Crafts Acylation; 1.5 h;
参考文献
Prescient NeuroPharma Inc.
Patent: US6699909 B1, 2004 ;
Location in patent: Page/Page column 28 ;
反应条件
carbon disulfide; aluminium trichloride
Behandeln des Reaktionsprodukts mit Eis und wss. Salzsaeure;
参考文献
v. Braun; Weissbach
Chemische Berichte, 1931 , vol. 64, p. 1785,1788
Full Text Show Details
Manske
Journal of the American Chemical Society, 1931 , vol. 53, p. 1104,1108
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Hey; Kohn
Journal of the Chemical Society, 1949 , p. 3177,3179
反应条件
1: KOH / ethanol / Heating
2: polyphosphoric acid / Heating
View Scheme
参考文献
Pramanik; Mukherjee
Journal of the Indian Chemical Society, 1997 , vol. 74, # 9 p. 734 - 735
反应条件
1: piperidine / 72 h / 30 - 40 °C
2: KOH / ethanol / Heating
3: polyphosphoric acid / Heating
View Scheme
参考文献
Pramanik; Mukherjee
Journal of the Indian Chemical Society, 1997 , vol. 74, # 9 p. 734 - 735
反应条件
aluminium trichloride; benzene
参考文献
Ali et al.
Journal of the Chemical Society, 1937 , p. 1013,1015
参考文献
Manske
Journal of the American Chemical Society, 1931 , vol. 53, p. 1104,1108
参考文献
Speight; Stevenson; Thorpe
Journal of the Chemical Society, 1924 , vol. 125, p. 2191
参考文献
Jackson; Kenner
Journal of the Chemical Society, 1928 , p. 578
Full Text Show Details
Speight; Stevenson; Thorpe
Journal of the Chemical Society, 1924 , vol. 125, p. 2191
参考文献
Jackson; Kenner
Journal of the Chemical Society, 1928 , p. 578
参考文献
Ali et al.
Journal of the Chemical Society, 1937 , p. 1013,1015
