3-(3,4-二甲基苯基)丙酸合成路线 (共 14 条)
反应条件
1: SOCl2 2: AlCl3 / CS2 View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 32, p. 4082 - 4098
反应条件
1: 97 percent / iron powder, bromine, iodidne / CH2Cl2 / Ambient temperature; overnight
2: 99 percent / 85percent phosphoric acid, P2O5 / 2 h / 90 °C
View Scheme
参考文献
Bartmann; Konz; Ruger
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 3 p. 677 - 682
反应条件
phosphoric acid; phosphorus pentoxide
T=90°C; 3 h;
参考文献
Bartmann; Konz; Ruger
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 3 p. 677 - 682
反应条件
1: 97 percent / iron powder, bromine, iodidne / CH2Cl2 / Ambient temperature; overnight
2: 99 percent / 85percent phosphoric acid, P2O5 / 2 h / 90 °C
3: 96 percent / ethyldiisopropylamine, H2 / 10percentPd on charcoal / ethanol / 0.17 h / Ambient temperature
View Scheme
参考文献
Fisnerova,L. et al.
Collection of Czechoslovak Chemical Communications, 1967 , vol. 32, p. 4082 - 4098