3-(1,3-苯并噻唑-2-基硫基)丙腈合成路线 （共 8 条）
反应条件
N-ethyl-N,N-diisopropylamine in acetone T=20°C; 0.5 h; Sonication;
参考文献
Deligeorgiev, Todor; Kaloyanova, Stefka; Lesev, Nedyalko; Vaquero, Juan J.
Ultrasonics Sonochemistry, 2010 , vol. 17, # 5 p. 783 - 788
反应条件
aluminium trichloride in chloroform T=40°C; 1 h;
参考文献
Anan'eva, K.V.; Rozhkov, N.K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 456 - 459
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 554 - 557
反应条件
N,N-dimethyl-formamide; trichlorophosphate T=90 - 100°C; 1 h;
参考文献
D'Amico, John J.; Suba, Lydia; Ruminski, Peter G.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1629 - 1635
反应条件
sodium hydroxide 1.) 50-60 deg C, 1d 2.) 25 - 30 deg C, 15 min;
参考文献
Deligeorgiev, Todor; Kaloyanova, Stefka; Lesev, Nedyalko; Vaquero, Juan J.
Ultrasonics Sonochemistry, 2010 , vol. 17, # 5 p. 783 - 788
反应条件
1: 88 percent / 1.), 2.) aq.NaOH / 1)50-60 deg C, 24h 2)25-30 deg C, 30min 2: 99 percent / POCl3, DMF / 1 h / 90 - 100 °C View Scheme
参考文献
D'Amico, John J.; Suba, Lydia; Ruminski, Peter G.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1629 - 1635
反应条件
aluminium trichloride in toluene 1 h; Heating;
参考文献
Anan'eva, K.V.; Rozhkov, N.K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 456 - 459
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 554 - 557
反应条件
sulfuric acid T=110°C; 5 h; different time, temperature, solvent; Product distribution;
参考文献
Anan'eva, K.V.; Rozhkov, N.K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 456 - 459
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 554 - 557
反应条件
hydrogenchloride derivatives with CN and CONH2 gived a same product;
参考文献
Anan'eva, K.V.; Rozhkov, N.K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 456 - 459
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 554 - 557
