6-甲基-2-苯基-喹喔啉合成路线 (共 19 条)
参考文献
Hinsberg
Justus Liebigs Annalen der Chemie, 1887 , vol. 237, p. 368
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Lellmann; Donner
Chemische Berichte, 1890 , vol. 23, p. 166,171
反应条件
gallium(III) perchlorate in ethanol
T=25°C;
参考文献
Pan, Fan; Chen, Tang-Ming; Cao, Jia-Jia; Zou, Jian-Ping; Zhang, Wei
Tetrahedron Letters, 2012 , vol. 53, # 20 p. 2508 - 2510
反应条件
in ethanol
2 h; Heating;
参考文献
Loriga, Mario; Nuvole, Antonio; Paglietti, Giuseppe
Journal of Chemical Research, Miniprint, 1989 , # 7 p. 1553 - 1566
反应条件
K3PO4*3H2O
T=40°C; 12 h;
参考文献
Lian, Mi; Li, Qi; Zhu, Yanping; Yin, Guodong; Wu, Anxin
Tetrahedron, 2012 , vol. 68, # 47 p. 9598 - 9605
反应条件
FeCl3·6H2O; sulfur in neat (no solvent)
T=120°C; 24 h; Inert atmosphere; Overall yield = 80 percent;
参考文献
Nguyen, Thanh Binh; Retailleau, Pascal; Al-Mourabit, Ali
Organic Letters, 2013 , vol. 15, # 20 p. 5238 - 5241
反应条件
silver hexafluoroantimonate; 6-methoxyquinoline N-oxide; PPh3 gold(I) chloro complex; bis-(trifluoromethylsulphonyl)amine in toluene
T=70°C; Sealed tube; Overall yield = 71 percent; Overall yield = 32 mg;
参考文献
Shi, Shuai; Wang, Tao; Yang, Weibo; Rudolph, Matthias; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 21 p. 6576 - 6580
反应条件
potassium carbonate in toluene
T=90°C; 8 h; Sealed tube; Overall yield = 82 percent;
参考文献
Song, Jinli; Li, Xiaolong; Chen, Yongxin; Zhao, Mingming; Dou, Yani; Chen, Baohua
Synlett, 2012 , vol. 23, # 16 art. no. ST-2012-W0450-L, p. 2416 - 2420
反应条件
in ethanol
1 h; Heating;
参考文献
Taylor, Edward C.; Maryanoff, Cynthia A.; Skotnicki, Jerauld S.
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2512 - 2515
反应条件
in acetonitrile
Heating;
参考文献
Rao, M Hanmantha; Reddy, A Pandu Ranga; Veeranagaiah, V
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 2 p. 88 - 91
反应条件
acetic acid in benzene
2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kano, Shinzo; Shibuya, Shiroshi; Yuasa, Yoko
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 6 p. 1559 - 1561