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乙二醇
甲醛
63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
252045-81-1
合成路线
(共 8 条)
625-95-6
3-碘甲苯
+
693-02-7
1-己炔
→
反应条件
252045-81-1
反应条件
potassium carbonate; triphenylphosphine; copper(l) iodide; cobalt palladium in water T=80°C; 6 h;
参考文献
Li, Yingguang; Zhou, Ping; Dai, Zhihui; Hu, Zhixin; Sun, Peipei; Bao, Jianchun
New Journal of Chemistry, 2006 , vol. 30, # 6 p. 832 - 837
591-17-3
3-溴甲基苯
+
693-02-7
1-己炔
→
反应条件
252045-81-1
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide T=90°C;
参考文献
Roesch; Larock
Journal of Organic Chemistry, 2001 , vol. 66, # 2 p. 412 - 420
625-95-6
3-碘甲苯
+
35864-20-1
→
反应条件
252045-81-1
反应条件
diphenylphosphine-based palladium(0) complex on MCM-41 in water; N,N-dimethyl-formamide T=60°C; Stille coupling; 8 h;
参考文献
Zhao, Hong; Zheng, Guomin; Hao, Wenyan; Cai, Mingzhong
Applied Organometallic Chemistry, 2010 , vol. 24, # 2 p. 92 - 98
591-17-3
3-溴甲基苯
+
35864-20-1
→
反应条件
252045-81-1
反应条件
MCM-41-supported mercapto palladium(0) complex in water; N,N-dimethyl-formamide T=60°C; Stille coupling; 16 h;
参考文献
Zhao, Hong; Zheng, Guomin; Hao, Wenyan; Cai, Mingzhong
Applied Organometallic Chemistry, 2010 , vol. 24, # 2 p. 92 - 98
693-02-7
1-己炔
→
反应条件
252045-81-1
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride T=50°C;
参考文献
Kang, Song Su; Yum, Eul Kgun; Sung, Nack-Do
Heterocycles, 2003 , vol. 60, # 12 p. 2727 - 2736
1197991-11-9
→
反应条件
1416562-64-5
+
252045-81-1
反应条件
1: triethylamine; tetrakis(triphenylphosphine) palladium(0); triphenylphosphine; copper(l) iodide / dichloromethane / 50 °C / |Inert atmosphere 2: p-toluidine View Scheme
参考文献
Danilkina; Gorbunova; Sorokoumov; Balova
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 11 p. 1424 - 1434
Zh. Org. Khim., 2012 , vol. 48, # 11 p. 1428 - 1439,12
693-02-7
1-己炔
→
反应条件
1416562-64-5
+
252045-81-1
反应条件
1: triethylamine; tetrakis(triphenylphosphine) palladium(0); triphenylphosphine; copper(l) iodide / dichloromethane / 50 °C / |Inert atmosphere 2: p-toluidine View Scheme
参考文献
Danilkina; Gorbunova; Sorokoumov; Balova
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 11 p. 1424 - 1434
Zh. Org. Khim., 2012 , vol. 48, # 11 p. 1428 - 1439,12
67-56-1
甲醇
+
1416562-59-8
→
反应条件
1416562-64-5
+
1416562-72-5
+
1416562-71-4
+
103-69-5
N-乙基苯胺
+
252045-81-1
反应条件
p-toluidine
参考文献
Danilkina; Gorbunova; Sorokoumov; Balova
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 11 p. 1424 - 1434
Zh. Org. Khim., 2012 , vol. 48, # 11 p. 1428 - 1439,12