5-(氯甲基)异邻苯二甲酸二甲酯合成路线 （共 4 条）
反应条件
thionyl chloride Chlorination; 1 h; Heating;
参考文献
Dimick, Sarah M.; Powell, Steven C.; McMahon, Stephen A.; Moothoo, Davina N.; Naismith, James H.; Toone, Eric J.
Journal of the American Chemical Society, 1999 , vol. 121, # 44 p. 10286 - 10296
反应条件
1: 95 percent / conc. H2SO4 / 24 h / Heating 2: 76 percent / 0.1 M aq. NaOH / methanol / 18 h 3: 88 percent / borane-methyl sulfide / tetrahydrofuran / 24 h / 27 °C 4: 93 percent / SOCl2 / 1 h / Heating View Scheme
参考文献
Dimick, Sarah M.; Powell, Steven C.; McMahon, Stephen A.; Moothoo, Davina N.; Naismith, James H.; Toone, Eric J.
Journal of the American Chemical Society, 1999 , vol. 121, # 44 p. 10286 - 10296
反应条件
1: 76 percent / 0.1 M aq. NaOH / methanol / 18 h 2: 88 percent / borane-methyl sulfide / tetrahydrofuran / 24 h / 27 °C 3: 93 percent / SOCl2 / 1 h / Heating View Scheme
参考文献
Dimick, Sarah M.; Powell, Steven C.; McMahon, Stephen A.; Moothoo, Davina N.; Naismith, James H.; Toone, Eric J.
Journal of the American Chemical Society, 1999 , vol. 121, # 44 p. 10286 - 10296
反应条件
1: 88 percent / borane-methyl sulfide / tetrahydrofuran / 24 h / 27 °C 2: 93 percent / SOCl2 / 1 h / Heating View Scheme
参考文献
Dimick, Sarah M.; Powell, Steven C.; McMahon, Stephen A.; Moothoo, Davina N.; Naismith, James H.; Toone, Eric J.
Journal of the American Chemical Society, 1999 , vol. 121, # 44 p. 10286 - 10296
