反应条件
1: 75 percent / RuCl3; NaIO4 / H2O; ethyl acetate / 0 - 20 °C 2: DIBAL-H / toluene / -78 °C 3: 2,6-lutidine 4: 0.33 h / Heating 5: Et3N / cyclohexane / 40 °C 6: 63 percent / Zn-Cu; NH4Cl / methanol / 20 °C 7: 62 percent / m-CPBA; NaHCO3 / CH2Cl2 / 0 °C 8: HCl; water / Heating View Scheme
参考文献
Miranda, Paulo Cesar M. L.; Correia, Carlos Roque D.
Tetrahedron Letters, 1999 , vol. 40, # 44 p. 7735 - 7738
