反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere 1.2: -78 - 20 °C 2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 30 °C / Inert atmosphere View Scheme
参考文献
Lindhardt, Anders T.; Simonssen, Roger; Taaning, Rolf H.; Gogsig, Thomas M.; Nilsson, Goeran N.; Stenhagen, Gunnar; Elmore, Charles S.; Skrydstrup, Troels
Journal of Labelled Compounds and Radiopharmaceuticals, 2012 , vol. 55, # 11 p. 411 - 418