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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
252316-67-9
合成路线
（共 7 条）
252316-67-9
→
反应条件
53463-68-6
10-溴-1-癸醇
反应条件
1: With [2,2']bipyridinyl; trimethylsilyl trifluoromethanesulfonate in dichloromethane T=0°C; 0.5 h; Inert atmosphere; 2: With water in diethyl ether; dichloromethane T=20°C; 7 h; Inert atmosphere; chemoselective reaction;
参考文献
Fujioka, Hiromichi; Minamitsuji, Yutaka; Kubo, Ozora; Senami, Kento; Maegawa, Tomohiro
Tetrahedron, 2011 , vol. 67, # 16 p. 2949 - 2960
109-87-5
甲缩醛
+
53463-68-6
10-溴-1-癸醇
→
反应条件
252316-67-9
反应条件
toluene-4-sulfonic acid; lithium bromide T=20°C; 5 h;
参考文献
Fujioka, Hiromichi; Minamitsuji, Yutaka; Kubo, Ozora; Senami, Kento; Maegawa, Tomohiro
Tetrahedron, 2011 , vol. 67, # 16 p. 2949 - 2960
13057-17-5
溴甲基甲基醚
+
53463-68-6
10-溴-1-癸醇
→
反应条件
252316-67-9
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=0 - 20°C;
参考文献
Tichy, Tomas; Andrei, Graciela; Dracinsky, Martin; Holy, Antonin; Balzarini, Jan; Snoeck, Robert; Krecmerova, Marcela
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 11 p. 3527 - 3539
112-43-6
10-十一烯-1-醇
→
反应条件
252316-67-9
反应条件
1: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 0 - 20 °C 2: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 3 h / 20 °C 3: sodium periodate / tetrahydrofuran; water / 1 h / 0 °C 4: sodium tetrahydroborate; water / tetrahydrofuran / 20 °C 5: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Tichy, Tomas; Andrei, Graciela; Dracinsky, Martin; Holy, Antonin; Balzarini, Jan; Snoeck, Robert; Krecmerova, Marcela
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 11 p. 3527 - 3539
7766-50-9
溴代十一碳烯
→
反应条件
252316-67-9
反应条件
1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 3 h / 20 °C 2: sodium periodate / tetrahydrofuran; water / 1 h / 0 °C 3: sodium tetrahydroborate; water / tetrahydrofuran / 20 °C 4: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Tichy, Tomas; Andrei, Graciela; Dracinsky, Martin; Holy, Antonin; Balzarini, Jan; Snoeck, Robert; Krecmerova, Marcela
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 11 p. 3527 - 3539
85920-81-6
10-溴癸醛
→
反应条件
252316-67-9
反应条件
1: sodium tetrahydroborate; water / tetrahydrofuran / 20 °C 2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Tichy, Tomas; Andrei, Graciela; Dracinsky, Martin; Holy, Antonin; Balzarini, Jan; Snoeck, Robert; Krecmerova, Marcela
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 11 p. 3527 - 3539
130203-52-0
→
反应条件
252316-67-9
反应条件
1: sodium periodate / tetrahydrofuran; water / 1 h / 0 °C 2: sodium tetrahydroborate; water / tetrahydrofuran / 20 °C 3: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Tichy, Tomas; Andrei, Graciela; Dracinsky, Martin; Holy, Antonin; Balzarini, Jan; Snoeck, Robert; Krecmerova, Marcela
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 11 p. 3527 - 3539
