10H-吩噻嗪-2-羧酸合成路线 （共 12 条）
反应条件
1: With iodine in pyridine T=20 - 100°C; 20.25 h; 2: With sodium hydroxide in water T=100°C; 1 h; 3: With hydrogenchloride in water
参考文献
Auvin, Serge; Chabrier De Lassauniere, Pierre-Etienne
Patent: US2005/222045 A1, 2005 ;
Location in patent: Page/Page column 11 ;
反应条件
1: AlCl3; CS2 2: aqueous NaClO View Scheme
参考文献
Massie et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1006
反应条件
hydrogenchloride; water in methanol T=100°C;
参考文献
Kubota, Katsumi; Kurebayashi, Hirotaka; Miyachi, Hirotaka; Tobe, Masanori; Onishi, Masako; Isobe, Yoshiaki
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 10 p. 2766 - 2771
反应条件
1: AlCl3; CS2 2: AlCl3; CS2 3: aqueous NaClO View Scheme
参考文献
Baltzly et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 2673,2677
反应条件
pyridine anschliessendes Erwaermen mit wss.-aethanol. NaOH;
参考文献
Schmitt et al.
Bulletin de la Societe Chimique de France, 1957 , p. 938,943, 944
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Massie et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 251
参考文献
Massie et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1006
反应条件
2: ethanolic KOH View Scheme
参考文献
Massie et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1006
反应条件
potassium carbonate; potassium iodide in acetone 24 h; Heating;
参考文献
Kadaba,P.K.
Journal of Heterocyclic Chemistry, 1966 , vol. 3, p. 345 - 347
反应条件
1: (i) PCl5, benzene, (ii) NH3 2: POCl3 / Heating View Scheme
参考文献
Craig,P.N. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1138 - 1143
反应条件
1: (i) PCl5, benzene, (ii) NH3 2: POCl3 / Heating 3: (i) NaNH2, toluene, (ii) /BRN= 506000/ View Scheme
参考文献
Craig,P.N. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1138 - 1143
