O,O-二乙基硫代磷酰氯合成路线 （共 132 条）
参考文献
Yadav, Veejendra K.; Balamurugan, Rengarajan; Parvez, Masood; Yamdagni, Raghav
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 3 p. 323 - 332
参考文献
Kabatschnik; Mastrjukowa
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 1924; engl. Ausg. S. 1867
反应条件
triethylamine T=130 - 140°C; 30 h;
参考文献
Vorob'eva, N. N.; Razvodovskaya, L. V.; Negrebetskii, V. V.; Grapov, A. F.; Mel'nikov, N. N.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 4 p. 781 - 786,688 - 693
反应条件
sodium hydride in tetrahydrofuran T=0 - 5°C; 12 h;
参考文献
Timperley, Christopher M.; Casey, Krystal E.; Notman, Stuart; Sellers, David J.; Williams, Nancy E.; Williams, Nichola H.; Williams, Gareth R.
Journal of Fluorine Chemistry, 2006 , vol. 127, # 12 p. 1554 - 1563
反应条件
in N,N-dimethyl-formamide
参考文献
Chavan, Vishal P.; Mane, Avinash S.; Shingare, Murlidhar S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 4 p. 339 - 341
反应条件
potassium hydroxide; ethanol
参考文献
Farbenfabr.Bayer
Patent: DE1083809 , 1957 ;
反应条件
potassium tert-butylate; tert-butyl alcohol
参考文献
Wolff; Burger
Journal of the American Chemical Society, 1957 , vol. 79, p. 1970
反应条件
in acetone 19 h; Heating;
参考文献
Fudala, Louise; Lewin, Anita H.
Journal of Labelled Compounds and Radiopharmaceuticals, 1998 , vol. 41, # 1 p. 81 - 84
反应条件
pyridine; chlorobenzene
参考文献
Mel'nikow; Chochlow
Zhurnal Obshchei Khimii, 1953 , vol. 23, p. 1357,1358; engl. Ausg. S. 1419, 1420
反应条件
4-(N,N-dimethlyamino)pyridine; N-benzyl-N,N,N-triethylammonium chloride; dodecanesulphonic acid sodium salt; potassium carbonate in water T=50°C; pH=9.5 - 10; 2.5 h; Reagent/catalystTemperatureTimepH-value;
参考文献
Ge, Xin; Qian, Chao; Chen, Xinzhi
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 739 - 744
