O,O-二乙基硫代磷酰氯合成路线 （共 132 条）
反应条件
4-(N,N-dimethlyamino)pyridine; potassium hydroxide in dichloromethane; water
参考文献
The Dow Chemical Company
Patent: US4814448 A1, 1989 ;
反应条件
copper; potassium carbonate in benzene byproducts: 4-aminosalicylic acid; raegents mixing in benzene, stiriing for 2 h, filtering and evapg.; detected by NMR spectrum and gas chromy.;
参考文献
Lecat, J. L.; Devaud, M.
Polyhedron, 1983 , vol. 2, p. 1087 - 1090
反应条件
1: in tetrahydrofuran T=-78°C; 2: With sulfur in tetrahydrofuran T=-33°C; 0.5 h;
参考文献
Stankiewicz, Marek; Nycz, Jacek; Rachon, Janusz
Heteroatom Chemistry, 2002 , vol. 13, # 4 p. 330 - 339
反应条件
potassium hydroxide in diethyl ether; ethanol
参考文献
GLENN, JR., ROBERT WAYNE
Patent: US2002/41855 A1, 2002 ;
反应条件
PEG-400; aluminum oxide; sodium hydroxide; water 1.) MeOH, r.t., 30 min, 2.) r.t., 1 h;
参考文献
Ramadas; Janarthanan; Meera Rani
Organic Preparations and Procedures International, 1998 , vol. 30, # 4 p. 469 - 472
参考文献
Farbenfabr. Bayer
Patent: DE814152 , 1948 ;
DRP/DRBP Org.Chem.
反应条件
in ethanol 1 h; Heating; Yield given;
参考文献
Terreni, Marco; Pregnolato, Massimo; Resnati, Giuseppe; Benfenati, Emilio
Tetrahedron, 1995 , vol. 51, # 29 p. 7981 - 7992
参考文献
McIvor et al.
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1819,1827
反应条件
das Natrium-Salz reagiert;
参考文献
McIvor et al.
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1819,1827
反应条件
copper; potassium carbonate in benzene byproducts: 4-aminosalicylic acid; raegents mixing in benzene, stiriing for 2 h, filtering and evapg.; detected by NMR spectrum and gas chromy.;
参考文献
Lecat, J. L.; Devaud, M.
Polyhedron, 1983 , vol. 2, p. 1087 - 1090
