O,O-二乙基硫代磷酰氯合成路线 （共 132 条）
反应条件
4-(N,N-dimethlyamino)pyridine; N-benzyl-N,N,N-triethylammonium chloride; dodecanesulphonic acid sodium salt; potassium carbonate in water T=50°C; pH=9.5 - 10; 2.5 h;
参考文献
Ge, Xin; Qian, Chao; Chen, Xinzhi
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 739 - 744
反应条件
PEG-400; aluminum oxide; sodium hydroxide; water 1.) MeOH, r.t., 30 min, 2.) r.t., 1 h;
参考文献
Ramadas; Janarthanan; Meera Rani
Organic Preparations and Procedures International, 1998 , vol. 30, # 4 p. 469 - 472
参考文献
Bakanowa,S.M. et al.
Organiceskie Insektofungicidy i Gerbicidy <Moskau 1955>Chem.Abstr., S.82,86 1959 , p. 6129
参考文献
Ponomarchuk, M. P.; Kasukhin, L. F.; Budilova, I. Yu.; Gololobov, Yu. G.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 9 p. 1937 - 1946,1561 - 1568
反应条件
triethylamine; isopropyl alcohol
参考文献
Dieng, Thierno; Fraix, Aurore; Salauen, Jean-Yves; Dez, Isabelle; Klein Gebbink, Robertus J. M.; Van Koten, Gerard; Jaffres, Paul-Alain
Synlett, 2008 , # 20 p. 3121 - 3124
反应条件
in tert-butyl alcohol T=50 - 60°C;
参考文献
Miller,B.
Tetrahedron, 1964 , vol. 20, p. 2069 - 2078
反应条件
triethylamine in diethyl ether
参考文献
Ryu,E.K.; Cates,L.A.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 1022
反应条件
1: O,O-diethyl chlorothiophosphate With ammonia; potassium in tetrahydrofuran T=-78°C; 2: With sulfur in tetrahydrofuran T=-33°C; 0.5 h; 3: methyl iodide in tetrahydrofuran T=20°C; 3 h;
参考文献
Stankiewicz, Marek; Nycz, Jacek; Rachon, Janusz
Heteroatom Chemistry, 2002 , vol. 13, # 4 p. 330 - 339
参考文献
Ryu,E.K.; Cates,L.A.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 1022
反应条件
triethylamine T=130 - 140°C; 30 h;
参考文献
Vorob'eva, N. N.; Razvodovskaya, L. V.; Negrebetskii, V. V.; Grapov, A. F.; Mel'nikov, N. N.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 4 p. 781 - 786,688 - 693
