二乙氧基-乙硫基-巯基膦烷合成路线 （共 46 条）
反应条件
thiamine diphosphate; diethylazodicarboxylate in benzene
T=50°C; 6 h;
参考文献
Mlotkowska, B.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 3 p. 380 - 386
反应条件
triethylamine; benzene
参考文献
Meinhardt; Vogel
Journal of Organic Chemistry, 1959 , vol. 24, p. 1604
参考文献
Khusainova; Mostovaya; Nizamov; Cherkasov
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 4 p. 581 - 582
反应条件
in water
The silver salt of O,O-diethyl dithiophosphate was prepared from equimolar aq. solns. of AgNO3 and NH4(1+){S2P(OEt)2}(1-) and reacted in situ with an aq. soln. of Et3TeI. The react. mixt. was wartmed up to 70°C for ca. 3 h.; React. mixt. cooled to room temp., Et3TeAg4I5 extd. with CH2Cl2 and pptd. with CHCl3; elem.anal.; Et2Te and EtSP(S)(OEt)2 detected in the extn. residue by MS.;
参考文献
Chadha, Raj K.
Inorganic Chemistry, 1988 , vol. 27, p. 1507 - 1510
参考文献
Norman et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 161
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Lubrizol Corp.
Patent: US2802856 , 1953 ;
反应条件
T=60 - 65°C; 7 h; Heating;
参考文献
Ofitserov, E. N.; Sinyashin, O. G.; Batyeva, E. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 4 p. 738 - 745,602 - 608
反应条件
4 A molecular sieve in diethyl ether
1 h; Ambient temperature;
参考文献
Aleshnikova, T. V.; Prokof'eva, A. F.; Manaev, S. A.; Negrebetskii, V. V.; Grapov, A. F.; Mel'nikov, N. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 4 p. 800 - 806,708 - 713
反应条件
in diethyl ether
Ambient temperatureother solvents; MechanismProduct distribution;
参考文献
Mikolajczyk, Marian; Kielbasinski, Piotr; Basinski, Wlodzimierz
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 899 - 908
反应条件
in 1,4-dioxane
30 h; Heating;
参考文献
Khusainova, N.G.; Sippel, I.Ya.; Berdnikov, E.A.; Pudovik, A.N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 11.1 p. 2460 - 2465,2284 - 2288
反应条件
in dichloromethane
mixing equimolar amts. of Pt{S2P(OEt)2} and dpm in CH2Cl2 at 25°C gave in fast reaction {(dpm)Pt{S2P(OEt)2}}(1+) and than slow (dpm)Pt{S2P(O)OEt} and EtS2P(OEt)2; identified by NMR;
参考文献
Colton, R.; Ebner, J.; Hoskins, B.F.
Inorganic Chemistry, 1988 , vol. 27, p. 1993 - 1999
