2,4-二羟基-6-甲基甲酸乙酯合成路线 (共 47 条)
反应条件
hydrogen; palladium on activated charcoal in sodium hydroxide P=760 Torr; 15 h; Ambient temperature;
参考文献
Gramatica, Paola; Gianotti, M. Pia; Speranza, Giovanna; Manitto, Paolo
Heterocycles, 1986 , vol. 24, # 3 p. 743 - 750
反应条件
Armillaria mellea iterative type I polyketide synthase ArmB, N-terminal hexahistidine-tagged protein in aq. phosphate buffer pH=7.4; 20 h; Enzymatic reaction;
参考文献
Chemistry and Biology, , vol. 20, # 9 p. 1101 - 1106
反应条件
n-butyllithium; sodium hydride in ethylene glycol dimethyl ether 8 h; Heatingother temperature, solvent, time; Product distribution;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277
反应条件
hydrogen; triethylamine; palladium on activated charcoal in methanol
参考文献
Gould; Cheng
Tetrahedron, 1993 , vol. 49, # 48 p. 11135 - 11144
反应条件
sodium hydride in tetrahydrofuran; hexane 1.) rt 30 min; 2.) rt 10 min, reflux 4 days;
参考文献
Leete, Edward; Michelson, Robert H.
Phytochemistry (Elsevier), 1989 , vol. 28, # 12 p. 3325 - 3330
反应条件
1: Br2 / acetic acid 2: Ni/Al, NaOH View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 44 p. 8171 - 8172
反应条件
1H-imidazole; n-butyllithium; sodium hydride in ethylene glycol dimethyl ether 24 h; Heating;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277
反应条件
1H-imidazole; n-butyllithium; sodium hydride in tetrahydrofuran; hexane 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2272 - 2277
反应条件
boron tribromide in dichloromethane 0.166667 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 4 p. 1043 - 1046
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane 24 h; Heating;
参考文献
Bruce, Ian; Spencer, Robert; Tyman, John
Journal of Chemical Research, Miniprint, 1992 , # 7 p. 1773 - 1795