4-(烯丙氧基)-1-溴苯合成路线 （共 36 条）
反应条件
T=223 - 230°C; Rearrangement; 2 h;
参考文献
Russell, Michael G.N.; Baker, Raymond; Ball, Richard G.; Thomas, Steven R.; Tsou, Nancy N.; Castro, Jose L.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 6 p. 893 - 899
反应条件
T=200°C; Isomerisierung; Rate constant;
参考文献
White et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 3271,3272
反应条件
T=185°C; Isomerisierung; Rate constant;
参考文献
Goering; Jacobson
Journal of the American Chemical Society, 1958 , vol. 80, p. 3277,3279
反应条件
tetrakis(triphenylphosphine) palladium(0); K3PO4*3H2O in water; N,N-dimethyl-formamide T=100°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Ran, Yan; Ma, Liang; Wang, Xuewei; Chen, Jinying; Wang, Guangcheng; Peng, Aihua; Chen, Lijuan
Molecules, 2012 , vol. 17, # 7 p. 8091 - 8104
反应条件
1: With magnesium in tetrahydrofuran T=20°C; 2 h; 2: With N,N-dimethyl-formamide in tetrahydrofuran T=0°C; 2 h; 3: With ammonia; iodine in tetrahydrofuran; water T=20°C; 2 h;
参考文献
Ishii, Genki; Harigae, Ryo; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2013 , vol. 69, # 5 p. 1462 - 1469
反应条件
tetrakis(triphenylphosphine) palladium(0); K3PO4*3H2O in water; N,N-dimethyl-formamide T=100°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Ran, Yan; Ma, Liang; Wang, Xuewei; Chen, Jinying; Wang, Guangcheng; Peng, Aihua; Chen, Lijuan
Molecules, 2012 , vol. 17, # 7 p. 8091 - 8104
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in water; isopropyl alcohol T=90°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Ran, Yan; Ma, Liang; Wang, Xuewei; Chen, Jinying; Wang, Guangcheng; Peng, Aihua; Chen, Lijuan
Molecules, 2012 , vol. 17, # 7 p. 8091 - 8104
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in water; isopropyl alcohol T=90°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Ran, Yan; Ma, Liang; Wang, Xuewei; Chen, Jinying; Wang, Guangcheng; Peng, Aihua; Chen, Lijuan
Molecules, 2012 , vol. 17, # 7 p. 8091 - 8104
反应条件
1: in N,N-dimethyl-formamide T=20°C; Suzuki coupling; 0.0833333 h; 2: With tetrakis(triphenylphosphine) palladium(0); K3PO4*3H2O in water; N,N-dimethyl-formamide T=100°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Molecules, , vol. 17, # 7 p. 8091 - 8104
反应条件
magnesium; iodine in tetrahydrofuran
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: EP1367060 A1, 2003 ;
Location in patent: Page 24 ;
