1-溴-2,5-二甲氧基苯合成路线 （共 45 条）
反应条件
(CH3)4Br in liquid sulphur dioxide T=-23°C; Rate constant;
参考文献
Helvetica Chimica Acta, , vol. 66, # 4 p. 1068 - 1077
参考文献
Tetrahedron Letters, , vol. 45, # 28 p. 5511 - 5514
反应条件
phosphorus pentabromide Erwaermen auf dem Dampfbad;
参考文献
Monatshefte fuer Chemie, , vol. 58, p. 92,104
参考文献
Chemische Berichte, , vol. 46, p. 1760
参考文献
Chemische Berichte, , vol. 58, p. 92,101
反应条件
diethylene glycol monoethyl ether; sodium amide in ethylene glycol dimethyl ether 1.) 45 deg C, 2 h, 2.) -10 deg C, 2 h, 3.) -30 deg C, 2 h;
参考文献
Synthetic Communications, , vol. 19, # 19 p. 3323 - 3330
反应条件
KNH2 1.) liq. NH3, 2.) 1 h; Yield given. Multistep reaction;
参考文献
Han, Yu Xin; Jovanovic, Misa V.; Biehl, Edward R.
Journal of Organic Chemistry, 1985 , vol. 50, # 8 p. 1334 - 1337
反应条件
cerium ammonium nitrate; silica gel in dichloromethane
参考文献
Ali, Mohammed Hashmat; Niedbalski, Melinda; Bohnert, Gary; Bryant, Daniel
Synthetic Communications, 2006 , vol. 36, # 12 p. 1751 - 1759
反应条件
boron trifluoride diethyl etherate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=-40°C; 1.5 h;
参考文献
Tohma, Hirofumi; Morioka, Hironori; Takizawa, Shinobu; Arisawa, Mitsuhiro; Kita, Yasuyuki
Tetrahedron, 2001 , vol. 57, # 2 p. 345 - 352
反应条件
5 Pd(II)/C(eggshell); sodium acetate in 1-methyl-pyrrolidin-2-one T=140°C; Heck reaction; 24 h;
参考文献
Cusati, Giuseppe; Wedig, Anja; Djakovitch, Laurent
Letters in Organic Chemistry, 2009 , vol. 6, # 1 p. 77 - 81
