2-碘-1,4-二甲氧基苯合成路线 （共 21 条）
反应条件
N-iodo-succinimide in acetonitrile T=20°C; 16 h;
参考文献
Carreno, M. Carmen; Garcia Ruano, Jose L.; Sanz, Gema; Toledo, Miguel A.; Urbano, Antonio
Tetrahedron Letters, 1996 , vol. 37, # 23 p. 4081 - 4084
反应条件
potassium carbonate in acetone Inert atmosphereReflux;
参考文献
Yamaguchi, Yoshihiro; Matsubara, Yoshio; Ochi, Takanori; Wakamiya, Tateaki; Yoshida, Zen-Ichi
Journal of the American Chemical Society, 2008 , vol. 130, # 42 p. 13867 - 13869
反应条件
1: AcOH; I2; HIO3 / H2SO4 / CCl4 / 48 h / Heating 2: aq. NaOH / 2-methyl-propan-2-ol / 6 h / Heating 3: K2CO3 / acetone / 12 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 14 p. 4504 - 4505
反应条件
1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; cobalt(II) dibromide in tetrahydrofuran; hexane T=0 - 20°C; 0.5 h; 2: With iodine in tetrahydrofuran; hexane T=20°C; 2 h; 3: With water; sodium thiosulfate in tetrahydrofuran; hexane
参考文献
Tetrahedron, , vol. 66, # 46 p. 8904 - 8910
反应条件
1: aq. NaOH / 2-methyl-propan-2-ol / 6 h / Heating 2: K2CO3 / acetone / 12 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 14 p. 4504 - 4505
反应条件
sulfuric acid Diazotization.man gibt die Diazoniumsulfatloesung zu einer waessr. Loesung von Kaliumjodid;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 332, p. 62
反应条件
in hexane; acetonitrile
反应条件
iodine cloride in acetic acid T=70°C; 4 h;
参考文献
Wariishi, Koji; Morishima, Sin-Ichi; Inagaki, Yoshio
Organic Process Research and Development, 2003 , vol. 7, # 1 p. 98 - 100
反应条件
sulfuric acid; iodine in acetonitrile T=0°C; 0.5 h; ElectrolysisFlow reactor; regioselective reaction;
参考文献
Organic Process Research and Development, , vol. 12, # 6 p. 1130 - 1136
反应条件
iodine cloride in dichloromethane T=25°C; 21 h; effect of reactant conc., solvent and salt effects; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 59, # 21 p. 6233 - 6244
