1-氮杂-2-甲氧基-1-环庚烯合成路线 （共 66 条）
反应条件
1: bis(acetylacetonate)nickel(II) / 24 h / 100 °C
2: methanol; sodium / 1 h / Reflux
View Scheme
参考文献
Josefik, Frantisek; Svobodova, Marketa; Bertolasi, Valerio; Simunek, Petr; MacHacek, Vladimir; Almonasy, Numan; Cernoskova, Eva
Journal of Organometallic Chemistry, 2012 , vol. 699, p. 75 - 81
参考文献
Fasseur, Dominique; Rigo, Benoit; Leduc, Catherine; Cauliez, Pascal; Couturier, Daniel
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1285 - 1291
反应条件
1: Heating
2: Zn dust, HCl, AcOH / 50 - 60 °C
View Scheme
参考文献
Jaen, Juan C.; Gregor, Vlad E.; Lee, Chet; Davis, Robert; Emmerling, Mark
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 6 p. 737 - 742
参考文献
C.H. Boehringer Sohn
Patent: DE944312 , 1953 ;
反应条件
in xylene
2 h; Heating;
参考文献
Nazarenko, Konstantin G.; Shyrokaya, Tatyana I.; Tolmachev, Andrei A.
Synthetic Communications, 2003 , vol. 33, # 2 p. 303 - 310
反应条件
in xylene
3 h; Heating;
参考文献
Nazarenko, Konstantin G.; Shyrokaya, Tatyana I.; Tolmachev, Andrei A.
Synthetic Communications, 2003 , vol. 33, # 2 p. 303 - 310
反应条件
in xylene
3 h; Heating;
参考文献
Nazarenko, Konstantin G.; Shyrokaya, Tatyana I.; Tolmachev, Andrei A.
Synthetic Communications, 2003 , vol. 33, # 2 p. 303 - 310
反应条件
in methanol
2 h; Ambient temperature;
参考文献
Dozorova, E. N.; Grizik, S. I.; Persianova, I. V.; Syubaev, R. D.; Shvarts, G. Ya.; Granik, V. G.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 2 p. 100 - 104
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 2 p. 154 - 158
反应条件
ammonium hydroxide; ammonia; copper(II) sulfate in water; toluene
参考文献
Warner-Lambert Company
Patent: US5486512 A1, 1996 ;
US 5486512 A
参考文献
Lettau; Buge; Harenberg; Hartel; Jarmer; Koch; Poppel; Schikora; Schneider; Weber; Nuhn
Pharmazie, 1993 , vol. 48, # 6 p. 410 - 414
