顺-1,4-二醋酸基-2-丁烯合成路线 （共 51 条）
反应条件
Grubb's 2nd generation catalyst in dichloromethane
T=20°C; 3 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Hryniewicka, Agnieszka; Kozlowska, Anna; Witkowski, Stanislaw
Journal of Organometallic Chemistry, 2012 , vol. 701, p. 87 - 92
反应条件
Cl2Ru=CHPh(PCy3)[bis(1,3-Mes-2-ylimidazolidine)] in dichloromethane
12 h; Heating;
参考文献
Chatterjee, Arnab K.; Choi, Tae-Lim; Sanders, Daniel P.; Grubbs, Robert H.
Journal of the American Chemical Society, 2003 , vol. 125, # 37 p. 11360 - 11370
反应条件
hydrogen; RhH(CO)(triphenylphosphine)3 in toluene
T=80°C; P=45004.5 Torr; 26.5 h; autoclaveInert atmosphere;
参考文献
DSM IP ASSETS B.V.; DE WILDEMAN, Stefaan, Marie, Andre; DE VRIES, Johannes, Gerardus; BOOGERS, Jeroen, Antonius, Franciscus
Patent: WO2012/116977 A1, 2012 ;
Location in patent: Page/Page column 4; 9 ;
反应条件
tris-(dibenzylideneacetone)dipalladium(0); N,O-bis-(trimethylsilyl)-acetamide; bis(diphenylphosphanyl)butane in dichloromethane
T=25°C; 1 h;
参考文献
Nomura, Nobuyoshi; Tsurugi, Ko; Okada, Masahiko
Angewandte Chemie - International Edition, 2001 , vol. 40, # 10 p. 1932 - 1935
反应条件
tris-(dibenzylideneacetone)dipalladium(0); N,O-bis-(trimethylsilyl)-acetamide; triphenylphosphine in dichloromethane
T=25°C; 10 h;
参考文献
Nomura, Nobuyoshi; Tsurugi, Ko; Okada, Masahiko
Angewandte Chemie - International Edition, 2001 , vol. 40, # 10 p. 1932 - 1935
反应条件
C55H58ClN3ORu; phenyl-trichloro-silane in toluene
T=50°C; 5 h;
参考文献
Behr, Arno; Gomes, Jessica Perez
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1 - 8
反应条件
C55H58ClN3ORu; phenyl-trichloro-silane in toluene
T=50°C; 5 h;
参考文献
Behr, Arno; Gomes, Jessica Perez
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1 - 8
反应条件
Grubb's 2nd generation catalyst in toluene
T=50°C; 5 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolventTemperatureTime;
参考文献
Kajetanowicz, Anna; Sytniczuk, Adrian; Grela, Karol
Green Chemistry, 2014 , vol. 16, # 3 p. 1579 - 1585
反应条件
tris-(dibenzylideneacetone)dipalladium(0); {4,6-bis(tert-butyl)-2-[3,5-bis(tert-butyl)-2-(dinapthyloxyphosphinoxy)-6-methylphenyl]-3-methylphenoxy}dinaphthyloxyphosphine
T=100°C; 1 h;
参考文献
MITSUBISHI CHEMICAL CORPORATION
Patent: US2004/147757 A1, 2004 ;
Location in patent: Page 31 ;
反应条件
C55H58ClN3ORu; phenyl-trichloro-silane in toluene
T=50°C; 5 h;
参考文献
Behr, Arno; Gomes, Jessica Perez
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1 - 8
