4-(丁基甲酰氨)苯基硼酸合成路线 (共 1 条)
反应条件
1: 4-(dihydroxyboryl)benzoic acid With N,N-diethanolaminomethyl polystyrene in tetrahydrofuran T=20°C; Solid phase reaction; 2 h; 2: N-butylamine With benzotriazol-1-ol; diisopropyl-carbodiimide in N,N-dimethyl-formamide T=20°C; Solid phase reaction; 6 h; 3: With water; acetic acid in tetrahydrofuran T=20°C; Solid phase reaction; 1 h;
参考文献
Hall, Dennis G.; Tailor, Jyoti; Gravel, Michel
Angewandte Chemie - International Edition, 1999 , vol. 38, # 20 p. 3064 - 3067