2-苯基-1,2-苯并噻唑-3-酮合成路线 （共 46 条）
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium carbonate; sulfur in N,N-dimethyl-formamide T=110°C; 3 h; Inert atmosphere;
参考文献
Bhakuni, Bhagat Singh; Balkrishna, Shah Jaimin; Kumar, Amit; Kumar, Sangit
Tetrahedron Letters, 2012 , vol. 53, # 11 p. 1354 - 1357
反应条件
sodium phosphate buffer in acetonitrile T=37°C; pH=7.5; 48 h;
参考文献
Sivaramakrishnan, Santhosh; Keerthi, Kripa; Gates, Kent S.
Journal of the American Chemical Society, 2005 , vol. 127, # 31 p. 10830 - 10831
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane T=195°C; 0.116667 h; Microwave irradiation;
参考文献
Liu, Dazhi; Tian, Zhen; Yan, Zhihui; Wu, Lixin; Ma, Yan; Wang, Quan; Liu, Wei; Zhou, Honggang; Yang, Cheng
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 11 p. 2960 - 2967
反应条件
1.1: trimethylaluminum / dichloromethane / 0 - 20 °C / Inert atmosphere 1.2: 60 °C / Inert atmosphere; Reflux 2.1: trifluoroacetic acid; bis-[(trifluoroacetoxy)iodo]benzene / dichloromethane View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 10 p. 3661 - 3668
反应条件
(i) Cl2, CCl4, (ii) /BRN= 605631/; Multistep reaction;
参考文献
Arzneimittel Forschung, , vol. 14, p. 1301 - 1306
反应条件
copper(l) iodide; oxygen in N,N-dimethyl-formamide T=70°C; P=760.051 Torr; 5 h;
参考文献
Wang, Zhen; Kuninobu, Yoichiro; Kanai, Motomu
Journal of Organic Chemistry, 2013 , vol. 78, # 14 p. 7337 - 7342
反应条件
1: 94 percent / sodium periodate / H2O; methanol / 2 h / 50 °C 2: 98 percent / thionyl chloride / CH2Cl2 / 0.17 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 4 p. 1183 - 1187
反应条件
in toluene 7 h; Reflux;
参考文献
Shimizu, Masao; Shimazaki, Teruaki; Yoshida, Tetsuya; Ando, Wataru; Konakahara, Takeo
Tetrahedron, 2012 , vol. 68, # 21 p. 3932 - 3936
反应条件
methyl iodide in methanol; acetone
参考文献
Sivaramakrishnan, Santhosh; Keerthi, Kripa; Gates, Kent S.
Journal of the American Chemical Society, 2005 , vol. 127, # 31 p. 10830 - 10831
反应条件
triethylamine in dichloromethane T=-15°C;
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
