2-苯基-1,2-苯并噻唑-3-酮合成路线 （共 46 条）
反应条件
sodium methylate in methanol 1 h; Heating;
参考文献
Shimizu, Masao; Sugano, Yoshinori; Konakahara, Takeo; Gama, Yasuo; Shibuya, Isao
Tetrahedron, 2002 , vol. 58, # 19 p. 3779 - 3783
反应条件
1: 211 mg / DCC; DMAP / tetrahydrofuran / 15 h / 25 °C 2: dimethyl dioxirane / acetone / 0 °C 3: 58 percent / methyl iodide / methanol; acetone View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 31 p. 10830 - 10831
反应条件
1: 96 percent / dimethyl dioxirane / acetone / 0.08 h / 0 °C 2: 88 percent / aq. sodium phosphate buffer / acetonitrile / 48 h / 37 °C / pH 7.5 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 31 p. 10830 - 10831
反应条件
1: dimethyl dioxirane / acetone / 0 °C 2: 58 percent / methyl iodide / methanol; acetone View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 31 p. 10830 - 10831
反应条件
1: 68.5 percent / DCC; DMAP / tetrahydrofuran / 12 h / 25 °C 2: 96 percent / dimethyl dioxirane / acetone / 0.08 h / 0 °C 3: 88 percent / aq. sodium phosphate buffer / acetonitrile / 48 h / 37 °C / pH 7.5 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 31 p. 10830 - 10831
反应条件
1: 20 percent / pyridine; phosphorous trichloride / 3 h / Heating 2: 56 percent / sodium phosphate buffer; aq. hydrogen peroxide / acetonitrile / 1.5 h / pH 7.4 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 31 p. 10830 - 10831
反应条件
thionyl chloride in dichloromethane 0.166667 h; Heating;
参考文献
Uchida, Yuzuru; Kozuka, Seizi
Journal of the Chemical Society, Chemical Communications, 1981 , # 11 p. 510 - 511
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Gopinath, Pushparathinam; Ramalingam, Krishnan; Muraleedharan, Kannoth Manheri; Karunagaran, Devarajan
MedChemComm, 2013 , vol. 4, # 4 p. 749 - 752
反应条件
1: 95 percent / AlMe3 / CH2Cl2; toluene / 0 - 60 °C 2: 71 percent / phenyliodine(III)-bis(trifluoroacetate); TFA / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Organic Letters, , vol. 8, # 21 p. 4811 - 4813
反应条件
1: thionyl chloride / Reflux 2: chlorine / tetrachloromethane / 20 °C 3: triethylamine / dichloromethane / -15 °C View Scheme
参考文献
Molecules, , vol. 15, # 11 p. 8214 - 8228
