2-苯基-1,2-苯并噻唑-3-酮合成路线 (共 46 条)
反应条件
1: 71 percent / pyridine / diethyl ether / 0.5 h / Heating 2: thionyl chloride, pyridine / CH2Cl2 / 3 h / 30 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 4 p. 1183 - 1187
反应条件
1: 94 percent / methanol / 3 h / Heating 2: 76 percent / sodium methoxide / methanol / 1 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 58, # 19 p. 3779 - 3783
反应条件
1: 71 percent / pyridine / diethyl ether / 0.5 h / Heating 2: thionyl chloride, pyridine / CH2Cl2 / 3 h / 30 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 4 p. 1183 - 1187
反应条件
1: 20 percent / thionyl chloride, pyridine / CH2Cl2 / 3 h / 30 °C 2: 94 percent / sodium periodate / H2O; methanol / 2 h / 50 °C 3: 98 percent / thionyl chloride / CH2Cl2 / 0.17 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 4 p. 1183 - 1187
反应条件
mercury(II) diacetate in acetic acid
参考文献
Chemische Berichte, , vol. 100, p. 2435 - 2444
反应条件
1: AcSH 2: Hg(OAc)2 / acetic acid View Scheme
参考文献
Chemische Berichte, , vol. 100, p. 2435 - 2444
反应条件
dihydrogen peroxide T=24.84°C; 72 h; aq. phosphate buffer;
参考文献
Dalton Transactions, , vol. 40, # 43 p. 11519 - 11529
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C 2: toluene / 7 h / Reflux View Scheme
参考文献
Tetrahedron, , vol. 68, # 21 p. 3932 - 3936
反应条件
1.1: trimethylaluminum / dichloromethane / 0 - 20 °C / Inert atmosphere 1.2: 60 °C / Inert atmosphere; Reflux 2.1: trifluoroacetic acid; bis-[(trifluoroacetoxy)iodo]benzene / dichloromethane View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 10 p. 3661 - 3668
反应条件
dihydrogen peroxide T=24.84°C; 72 h; aq. phosphate buffer;
参考文献
Dalton Transactions, , vol. 40, # 43 p. 11519 - 11529