1: H2; 20 percent Pd(OH)2/C / methanol; acetic acid / 75 h / 20 °C / 2585.74 Torr 2: 93 percent / 0.6 N aq. NaOH / 20 h / 4 °C 3: 79 percent / triethylamine; isopropenyl chloroformate / tetrahydrofuran / 1.25 h / 0 - 20 °C View Scheme
参考文献
Soucy, Francois; Grenier, Louis; Behnke, Mark L.; Destree, Antonia T.; McCormack, Teresa A.; Adams, Julian; Plamondon, Louis
Journal of the American Chemical Society, 1999 , vol. 121, # 43 p. 9967 - 9976
1: H2; 20 percent Pd(OH)2/C / methanol; acetic acid / 75 h / 20 °C / 2585.74 Torr
2: 93 percent / 0.6 N aq. NaOH / 20 h / 4 °C
View Scheme
参考文献
Soucy, Francois; Grenier, Louis; Behnke, Mark L.; Destree, Antonia T.; McCormack, Teresa A.; Adams, Julian; Plamondon, Louis
Journal of the American Chemical Society, 1999 , vol. 121, # 43 p. 9967 - 9976
