1.1: IPy2BF4 / acetonitrile / 12 h / -40 °C 1.2: LiAlH4 / tetrahydrofuran / 25 °C 2.1: HCl / tetrahydrofuran; H2O / 2 h / 25 °C 3.1: Jones reagent / acetone / 6 h / 0 - 25 °C 4.1: 42 mg / HCl / H2O / 48 h / 100 °C View Scheme
参考文献
Avenoza, Alberto; Busto, Jesus H.; Corzana, Francisco; Peregrina, Jesus M.; Sucunza, David; Zurbano, Maria M.
Tetrahedron Asymmetry, 2004 , vol. 15, # 4 p. 719 - 724
1: 96 percent / hydrogen / palladium on carbon / ethyl acetate / 12 h / 20 °C 2: 93 percent / water; Sc(OTf)3 / acetonitrile / 24 h / 25 °C 3: Jones reagent / acetone / 6 h / 0 - 20 °C View Scheme
参考文献
Avenoza, Alberto; Cativiela, Carlos; Corzana, Francisco; Peregrina, Jesus M.; Zurbano, Maria M.
Journal of Organic Chemistry, 1999 , vol. 64, # 22 p. 8220 - 8225
