乙基5-(4-甲氧基苯基)-5-氧代戊酸酯合成路线 (共 11 条)
反应条件
bis-triphenylphosphine-palladium(II) chloride T=20°C;
参考文献
Nambu, Hisanori; Hata, Kayoko; Matsugi, Masato; Kita, Yasuyuki
Chemistry - A European Journal, 2005 , vol. 11, # 2 p. 719 - 727
反应条件
aluminium trichloride in 1,1,2,2-tetrachloroethylene T=0°C; 3 h;
参考文献
Sakuragi; Tokumaru; Itoh; Terakawa; Kikuchi; Caldwell; Hsu
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 4 p. 1049 - 1057
反应条件
1: 68 percent / 2,2'-azobis[2-(2-imidazolin-2-yl)propane] dihydrochloride; cetyltrimethylammonium bromide / H2O / 24 h / 50 °C 2: 90 percent / [PdCl2(PPh)2] / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 11, # 2 p. 719 - 727
反应条件
1: aluminium chloride; nitrobenzene 2: sulfuric acid; ethanol View Scheme
参考文献
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, , vol. 15/5 A, p. 19
反应条件
1: 68 percent 2: 26 percent / AlCl3 / tetrachloroethene / 3 h / 0 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 4 p. 1049 - 1057
反应条件
1.1: magnesium / diethyl ether / |Reflux 1.2: 0 °C 2.1: sulfuric acid / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 8 p. 3647 - 3654
反应条件
sulfuric acid T=20°C;
参考文献
Guijarro, David; Pablo, Oscar; Yus, Miguel
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3647 - 3654
反应条件
ethanol; sulfuric acid
参考文献
Journal of the Indian Chemical Society, , vol. 17, p. 573,575
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, , vol. 15/5 A, p. 19
反应条件
1: aluminium chloride; nitrobenzene 2: sulfuric acid; ethanol View Scheme
参考文献
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, , vol. 15/5 A, p. 19
反应条件
1: potassium tert-butylate; tert-butyl alcohol / Erwaermen des Reaktionsprodukts mit wss. NaOH
2: Raney nickel; aqueous NaOH
View Scheme
参考文献
Johnson et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 2395,2400