253185-03-4合成路线 （共 388 条）
反应条件
hydrogen fluoride; boron trifluoride; dihydrogen peroxide T=-60°C; 0.5 h; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 46, # 21 p. 4305 - 4306
反应条件
helium; oxygen T=-30°C; P=4 Torr; 2 h; Product distributionRate constant;
参考文献
Zadok, Elazar; Sialom, Bonita; Mazur, Yehuda
Angewandte Chemie, 1980 , vol. 92, # 12 p. 1037 - 1038
反应条件
T=0 - 5°C; Bromierung;
参考文献
Hennion; Anderson
Journal of the American Chemical Society, 1944 , vol. 66, p. 1801
Journal of the American Chemical Society, 1946 , vol. 68, p. 424
反应条件
T=30 - 75°C; auch nach Zusatz von Perchlorsaeure sowie von Eisen(III)-chlorid; Rate constant;
参考文献
Parker et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 323,326
反应条件
iodine; 3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 0.166667 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
1: trifluoromethylsulfonic anhydride With urea hydrogen peroxide addition compound in dichloromethane; 2,2,2-trifluoroethanol T=0°C; 0.5 h; 2: 1-tert-butyl-4-iodobenzene in dichloromethane; 2,2,2-trifluoroethanol T=0°C; 3: tert-butyl benzene in dichloromethane; 2,2,2-trifluoroethanol T=0 - 20°C;
参考文献
Merritt, Eleanor A.; Malmgren, Joel; Klinke, Felix J.; Olofsson, Berit
Synlett, 2009 , # 14 p. 2277 - 2280
反应条件
1: AlCl3 / 45 °C 2: glacial acetic acid; acetic acid anhydride; HNO3 / 30 - 40 °C 3: nickel; isopropyl alcohol / 100 °C / 58840.6 Torr / Hydrogenation View Scheme
参考文献
Legge
Journal of the American Chemical Society, 1947 , vol. 69, p. 2079,2083
反应条件
1: 1.) AlCl3, 2.) AlCl3 / 1.) room temperature, 19 h 2: 67 percent / HNO3 / acetic anhydride; acetic acid / 50 h / Ambient temperature 3: 56 percent / 5percent sodium amalgam / methanol / 5 h / Heating View Scheme
参考文献
Okada, Tadashi; Karaki, Ichiro; Mataga, Noboru
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7191 - 7195
反应条件
1: diluted aqueous nitric acid / 200 - 350 °C 2: aqueous alkaline KMnO4 View Scheme
参考文献
Duffin et al.
Journal of the Chemical Society, 1959 , p. 2734,2740
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 24 h; Reagent/catalyst; Overall yield = 68 percent; Overall yield = 146.2 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
