253185-03-4合成路线 (共 388 条)
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22306-30-51,1,4,4,5,5,8,8-八甲基-1,2,3,4,5,6,7,8-八氢蒽+
反应条件
aluminium trichloride in pentane 0.666667 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 25, p. 708 - 711
反应条件
[Me3Si-H-SiMe3][B(C6F5)4] T=20°C; Friedel Crafts alkylation; 3 h;
参考文献
Journal of the American Chemical Society, , vol. 133, # 51 p. 21016 - 21027
反应条件
aluminium trichloride
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2079,2083
反应条件
T=20 - 80°C; Friedel Crafts alkylation;
参考文献
Journal of the American Chemical Society, , vol. 133, # 51 p. 21016 - 21027
反应条件
aluminum tri-bromide T=-0.1 - 99.9°C; Equilibrium constantThermodynamic data;
参考文献
Russian Journal of Physical Chemistry, , vol. 58, # 2 p. 297 - 298
Zhurnal Fizicheskoi Khimii, , vol. 58, # 2 p. 491 - 493
参考文献
Bulletin de la Societe Chimique de France, , p. 1238
反应条件
1.1: 100 percent / Br2; I2 / 0 °C 2.1: n-BuLi / tetrahydrofuran / 3 h / -78 - -45 °C 2.2: tributyl borate / tetrahydrofuran / -78 - 20 °C 2.3: 90 percent / Acid hydrolysis View Scheme
参考文献
Balaganesan, Banumathy; Shen, Wen-Jian; Chen, Chin H.
Tetrahedron Letters, 2003 , vol. 44, # 30 p. 5747 - 5750
参考文献
Sandoz Ltd.
Patent: US4464180 A1, 1984 ;
反应条件
1: iodine; dipotassium peroxodisulfate 2: potassium carbonate / acetonitrile / 24 h / 50 °C View Scheme
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188