253185-03-4合成路线 （共 388 条）
反应条件
1: 40 g / nitric and sulphuric acid / 0.25 h / 47 °C 2: 33.2 g / Na2S*9H2O, sulphur / H2O / 1.5 h / Heating 3: 28.5 g View Scheme
参考文献
Murphy, J. Timothy; Ridd, John H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 1767 - 1772
反应条件
lithium; ethylamine; diethylamine 40 h;
参考文献
Baggett, Neil; Mosihuzzaman, Mohammed; Webber, John M.
Carbohydrate Research, 1985 , vol. 136, p. 347 - 356
反应条件
ammonia; sodium in methanol T=-75 - -33°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Beger, J.; Thomas, B.; Vogel, T.; Kirmse, K.; Lang, R.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 3 p. 481 - 488
反应条件
calcium; ammonium chloride 1.) methylamine, ethylenediamine, 22h, 2.) 0 deg C, diethyl ether; Yield given. Yields of byproduct given;
参考文献
Benkeser, Robert A.; Belmonte, Frank G.; Kang, Jahyo
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2796 - 2802
反应条件
4 Aequivalente Lithium;
参考文献
Benkeser et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 854
反应条件
6 Aequivalente Lithium;
参考文献
Benkeser et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 854
反应条件
1: (i) HCl, (ii) /BRN= 3587243/, DMSO, (iii) /BRN= 1718733/, H2SO4 2: NH2OH*HCl, NaOMe / methanol / Heating View Scheme
参考文献
Buu-Hoi,N.P. et al.
Chimica Therapeutica, 1967 , vol. 2, p. 39 - 48
反应条件
1: 92 percent / H2SO4; HNO3 / H2O / 0 - 20 °C 2: H2 / Pd/C / ethyl acetate View Scheme
参考文献
Murphy, J. Timothy; Ridd, John H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 1767 - 1772
反应条件
aluminium trichloride in nitromethane
参考文献
Farmer, Luc J.; Marron, Kristen S.; Canan Koch, Stacie S.; Hwang; Kallel, E. Adam; Zhi, Lin; Nadzan, Alex M.; Robertson, Dave W.; Bennani, Youssef L.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 9 p. 2352 - 2356
参考文献
Eisenbraun,E.J. et al.
Journal of Organic Chemistry, 1968 , vol. 33, p. 2000 - 2008
