253185-03-4合成路线 (共 388 条)
反应条件
1: tetrachloromethane; iron (III)-chloride; chlorine 2: iron (III)-bromide; bromine View Scheme
参考文献
Lerer et al.
Bulletin de la Societe Chimique de France, 1957 , p. 173,180
反应条件
MnTPPCl; iodosylbenzene in water 12 h; other oxidant, MnIIITPPN3-catalyst; Product distribution;
参考文献
Smegal, John A.; Hill, Craig L.
Journal of the American Chemical Society, 1983 , vol. 105, # 11 p. 3515 - 3521
反应条件
T=190 - 245°C; Irradiation;
参考文献
Backhurst et al.
Journal of the Chemical Society, 1959 , p. 2742,2744
反应条件
1: AlCl3 2: AlCl3; 1,2-dichloro-ethane View Scheme
参考文献
Givaudan and Cie.
Patent: DE951267 , 1954 ;
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Givaudan Corp.
Patent: US2897237 , 1953 ;
反应条件
1: (bromination) 2: (i) Mg, (ii) /BRN= 1900390/ 3: SOCl2 View Scheme
参考文献
Akkerman,O.S.
Recueil des Travaux Chimiques des Pays-Bas, 1967 , vol. 86, p. 1018 - 1024
反应条件
1: 70 percent / HNO3, H2SO4 2: 86 percent / aq. sodium sulfide, sulfur 3: 1.) conc. HCl, aq. NaNO2, 2.) aq. KCN / 1.) EtOH, 0 deg C, 10 min, 2.) EtOH, 100 deg C, 15 min 4: SnCl2*2H2O / ethanol / 0.75 h / Heating View Scheme
参考文献
Atwal, Karnail S.; Ferrara, Francis N.; Ding, Charles Z.; Grover, Gary J.; Sleph, Paul G.; Dzwonczyk, Steven; Baird, Anne J.; Normandin, Diane E.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 1 p. 304 - 313
反应条件
1: tert-butyl benzene With n-butyllithium; potassium tert-butylate in hexane T=25°C; 2 h; 2: diazomethane; carbon dioxide in diethyl ether
参考文献
Baston, Eckhard; Maggi, Raimondo; Friedrich, Kirstin; Schlosser, Manfred
European Journal of Organic Chemistry, 2001 , # 21 p. 3985 - 3989
参考文献
Benkeser,R.A. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 4366 - 4370
反应条件
carbon disulfide; aluminium trichloride
参考文献
Bergmann; Szmuszkowicz
Journal of the American Chemical Society, 1948 , vol. 70, p. 2748,2750
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Hughes; Ingold; Taher
Journal of the Chemical Society, 1940 , p. 949,954
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Bachmann; Carlson; Moran
Journal of Organic Chemistry, 1948 , vol. 13, p. 916,920
反应条件
aluminium trichloride
参考文献
Brown; Marino
Journal of the American Chemical Society, 1959 , vol. 81, p. 5611,5612