in water
byproducts: BaSO4; aq. soln. of Mn-compd. mixed with excess of Ba-compd., addn. of sulfuric acid soln. (5percent v/v); filtered twice (Celite), recrytsd. twice (MeOH), washed (ether), dried (vac.);
参考文献
Radnai, Tamas; Ishiguro, Shin-ichi; Ohtaki, Hitoshi
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 5 p. 1445 - 1452
in acetone
molar ratio of manganese(II) salt:KSCN=1:2;
参考文献
Eristavi, D. I.; Tsintsadze, G. V.; Kereselidze, L. B.
Soobshcheniya Akademii Nauk Gruzinskoi SSR, 1970 , vol. 59, p. 57 - 59
C.A., 1970 , vol. 73, p. 136860
in ethanol
byproducts: KNO3; by mixing concd. solns. of KNCS and hydrated metal nitrate in hot EtOH in 2:1 mol ratio; cooling in the fridge overnight; the pptd. KNO3 was filtered;
参考文献
Goodgame, David M.L.; Lickiss, Paul D.; Rooke, Stephanie J.; White, Andrew J.P.; Williams, David J.
Inorganica Chimica Acta, 2003 , vol. 343, p. 61 - 73